O-(2,3,4-tri-O-benzyl-α-D-galactopyranosyl)-(1-3)-1,2,4,5,6-penta-O-benzyl-sn-myo-inositol

Base Information

Chemical Name:O-(2,3,4-tri-O-benzyl-α-D-galactopyranosyl)-(1-3)-1,2,4,5,6-penta-O-benzyl-sn-myo-inositol
CAS No.:319918-45-1
Molecular Formula:C₆₈H₇₀O₁₁
Molecular Weight:1063.3
Hs Code.:

Synonyms:O-(2,3,4-tri-O-benzyl-α-D-galactopyranosyl)-(1-3)-1,2,4,5,6-penta-O-benzyl-sn-myo-inositol

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Chemical Property of O-(2,3,4-tri-O-benzyl-α-D-galactopyranosyl)-(1-3)-1,2,4,5,6-penta-O-benzyl-sn-myo-inositol

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Technology Process of O-(2,3,4-tri-O-benzyl-α-D-galactopyranosyl)-(1-3)-1,2,4,5,6-penta-O-benzyl-sn-myo-inositol

There total 4 articles about O-(2,3,4-tri-O-benzyl-α-D-galactopyranosyl)-(1-3)-1,2,4,5,6-penta-O-benzyl-sn-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 319918-39-3
O-(6-O-allyl-2,3,4-tri-O-benzyl-α-D-galactopyranosyl)-(1-3)-1,2,4,5,6-penta-O-benzyl-sn-myo-inositol

: 319918-45-1
O-(2,3,4-tri-O-benzyl-α-D-galactopyranosyl)-(1-3)-1,2,4,5,6-penta-O-benzyl-sn-myo-inositol

Guidance literature:: With sodium acetate; palladium dichloride; In water; acetic acid; at 65 ℃; for 4h;
DOI:10.1246/bcsj.73.2521

Reference yield: 69.0%

: O-(6-O-p-nitrophenylsulfonyl-2,3,4-tri-O-benzyl-α-D-galactopyranosyl)-(1-3)-1,2,4,5,6-penta-O-benzyl-sn-myo-inositol

: 319918-45-1
O-(2,3,4-tri-O-benzyl-α-D-galactopyranosyl)-(1-3)-1,2,4,5,6-penta-O-benzyl-sn-myo-inositol

Guidance literature:: With tetrabutylammonium acetate; In N,N-dimethyl-formamide; at 80 ℃; for 6h;
DOI:10.1246/bcsj.73.2521

Reference yield:

: 26277-05-4
1,2,4,5,6-penta-O-benzyl-sn-myo-inositol

: 319918-45-1
O-(2,3,4-tri-O-benzyl-α-D-galactopyranosyl)-(1-3)-1,2,4,5,6-penta-O-benzyl-sn-myo-inositol

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / p-nitrobenzenesulfonyl chloride; silver trifluoromethanesulfonate; N,N-dimethylacetamide / CH₂Cl₂

2: 83 percent / CH₃COONa / PdCl₂ / acetic acid; H₂O / 4 h / 65 °C

With N,N-dimethyl acetamide; sodium acetate; silver trifluoromethanesulfonate; 4-Nitrobenzenesulfonyl chloride; palladium dichloride; In dichloromethane; water; acetic acid;
DOI:10.1246/bcsj.73.2521