Technology Process of C24H35N3O8
There total 3 articles about C24H35N3O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: copper(ll) sulfate pentahydrate; ascorbic acid / water; N,N-dimethyl-formamide / 0.75 h / 20 °C / Inert atmosphere
2: potassium carbonate; methanol / 20 °C
With
methanol; copper(ll) sulfate pentahydrate; potassium carbonate; ascorbic acid;
In
water; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2012.08.001
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 0.08 h / Reflux; Inert atmosphere
1.2: 2 h / 70 - 80 °C / Inert atmosphere
2.1: hydrogenchloride; sodium nitrite / water; acetone / 0 °C
2.2: 5 °C
3.1: copper(ll) sulfate pentahydrate; ascorbic acid / water; N,N-dimethyl-formamide / 0.75 h / 20 °C / Inert atmosphere
4.1: potassium carbonate; methanol / 20 °C
With
hydrogenchloride; methanol; copper(ll) sulfate pentahydrate; potassium carbonate; ascorbic acid; sodium nitrite;
In
water; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.carres.2012.08.001