1-(4-methoxyphenyl)-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexane

Base Information

Chemical Name:1-(4-methoxyphenyl)-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexane
CAS No.:1240790-33-3
Molecular Formula:C₁₉H₃₁BO₃
Molecular Weight:318.264
Hs Code.:

Synonyms:1-(4-methoxyphenyl)-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4-methoxyphenyl)-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexane

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Technology Process of 1-(4-methoxyphenyl)-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexane

There total 2 articles about 1-(4-methoxyphenyl)-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 154820-94-7
2-(hex-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 696-62-8
para-iodoanisole

: 1240790-33-3
1-(4-methoxyphenyl)-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexane

Guidance literature:: 2-(hex-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; With potassium fluoride; diethoxymethylsilane; nickel(II) bromide diethylene glycol dimethyl ether; 2-[4,5-dihydro-1,3-oxazol-2-yl]pyridine; potassium iodide; In N,N-dimethyl acetamide; at 25 ℃; for 0.0166667h; Glovebox; Inert atmosphere;

para-iodoanisole; In N,N-dimethyl acetamide; at 25 ℃; for 24h; regioselective reaction; Sealed tube; Inert atmosphere;
DOI:10.1002/anie.201907045

Reference yield: 79.0%

: 104-92-7
1-bromo-4-methoxy-benzene

: 2,2'-(hexane-1,1-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

: 1240790-33-3
1-(4-methoxyphenyl)-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexane

Guidance literature:: With KOH; bis(tri-t-butylphosphine)palladium⁽⁰⁾; In 1,4-dioxane; water; 5 mol% Pd-complex, 4.5 equiv of KOH, H2O/dioxane, 25°C, 6-24 h;
DOI:10.1021/ja105176v