allyl 3-N-(benzyloxycarbonyl)aminophenyl ether

Base Information

Chemical Name:allyl 3-N-(benzyloxycarbonyl)aminophenyl ether
CAS No.:515163-29-8
Molecular Formula:C₁₇H₁₇NO₃
Molecular Weight:283.327
Hs Code.:

Synonyms:allyl 3-N-(benzyloxycarbonyl)aminophenyl ether

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Chemical Property of allyl 3-N-(benzyloxycarbonyl)aminophenyl ether

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Technology Process of allyl 3-N-(benzyloxycarbonyl)aminophenyl ether

There total 5 articles about allyl 3-N-(benzyloxycarbonyl)aminophenyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 19972-88-4
3-Hydroxycarbanilic Acid Benzyl Ester

: 106-95-6
allyl bromide

: 515163-29-8
allyl 3-N-(benzyloxycarbonyl)aminophenyl ether

Guidance literature:: With potassium carbonate; In acetone; at 20 ℃; for 24h;
DOI:10.3987/com-02-s27

Reference yield:

: 554-84-7
meta-nitrophenol

: 515163-29-8
allyl 3-N-(benzyloxycarbonyl)aminophenyl ether

Guidance literature:: Multi-step reaction with 5 steps

1: 82 percent / TsOH*H₂O / benzene / 1 h / 50 °C

2: hydrogen / 10 percent Pd/C / ethanol / 4 h / 20 °C / 760 Torr

3: 14.39 g / CHCl₃ / 2 h / 20 °C

4: 75 percent / TsOH*H₂O / methanol / 1 h / Heating

5: 98 percent / K₂CO₃ / acetone / 24 h / 20 °C

With hydrogen; potassium carbonate; toluene-4-sulfonic acid; palladium on activated charcoal; In methanol; ethanol; chloroform; acetone; benzene;
DOI:10.3987/com-02-s27

Reference yield:

: 28659-20-3
3-(2-tetrahydropyranyloxy)nitrobenzene

: 515163-29-8
allyl 3-N-(benzyloxycarbonyl)aminophenyl ether

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen / 10 percent Pd/C / ethanol / 4 h / 20 °C / 760 Torr

2: 14.39 g / CHCl₃ / 2 h / 20 °C

3: 75 percent / TsOH*H₂O / methanol / 1 h / Heating

4: 98 percent / K₂CO₃ / acetone / 24 h / 20 °C

With hydrogen; potassium carbonate; toluene-4-sulfonic acid; palladium on activated charcoal; In methanol; ethanol; chloroform; acetone;
DOI:10.3987/com-02-s27