1,1-dimethylethyl (S)-1-[(S)-3-methyl-1-oxo-1-(2-oxo-3-oxazolidinyl)butan-2-ylamino]-1-oxo-3-phenylpropan-2-ylcarbamate

Base Information

• Chemical Name: 1,1-dimethylethyl (S)-1-[(S)-3-methyl-1-oxo-1-(2-oxo-3-oxazolidinyl)butan-2-ylamino]-1-oxo-3-phenylpropan-2-ylcarbamate
• CAS No.: 1008131-70-1
• Molecular Formula: C₂₂H₃₁N₃O₆
• Molecular Weight: 433.505

Synonyms:1,1-dimethylethyl (S)-1-[(S)-3-methyl-1-oxo-1-(2-oxo-3-oxazolidinyl)butan-2-ylamino]-1-oxo-3-phenylpropan-2-ylcarbamate

Chemical Property of 1,1-dimethylethyl (S)-1-[(S)-3-methyl-1-oxo-1-(2-oxo-3-oxazolidinyl)butan-2-ylamino]-1-oxo-3-phenylpropan-2-ylcarbamate

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Technology Process of 1,1-dimethylethyl (S)-1-[(S)-3-methyl-1-oxo-1-(2-oxo-3-oxazolidinyl)butan-2-ylamino]-1-oxo-3-phenylpropan-2-ylcarbamate

There total 1 articles about 1,1-dimethylethyl (S)-1-[(S)-3-methyl-1-oxo-1-(2-oxo-3-oxazolidinyl)butan-2-ylamino]-1-oxo-3-phenylpropan-2-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C2HF3O2*C8H14N2O3 + N-tert-butoxycarbonyl-L-phenylalanine (13734-34-4) → 1,1-dimethylethyl (S)-1-[(S)-3-methyl-1-oxo-1-(2-oxo-3-oxazolidinyl)butan-2-ylamino]-1-oxo-3-phenylpropan-2-ylcarbamate (1008131-70-1)

Guidance literature:

With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 48h;

DOI:10.1021/jo702286b

Reference yield: 68.0%

1,1-dimethylethyl (S)-1-[(S)-3-methyl-1-oxo-1-(2-oxo-3-oxazolidinyl)butan-2-ylamino]-1-oxo-3-phenylpropan-2-ylcarbamate (1008131-70-1) + N-tert-Butylacrylamide (107-58-4,25267-41-8) → 1,1-dimethylethyl (S)-1-[(S)-7-(1,1-dimethylethan-1-ylamino)-2-methyl-4,7-dioxoheptan-3-ylamino]-1-oxo-3-phenylpropan-2-ylcarbamate (1008131-80-3)

Guidance literature:

With samarium diiodide; water; In tetrahydrofuran; at -78 ℃; for 48h;

DOI:10.1021/jo702286b

Reference yield:

1,1-dimethylethyl (S)-1-[(S)-3-methyl-1-oxo-1-(2-oxo-3-oxazolidinyl)butan-2-ylamino]-1-oxo-3-phenylpropan-2-ylcarbamate (1008131-70-1) + trifluoroacetic acid (76-05-1) → C2HF3O2*C17H23N3O4

Guidance literature:

In dichloromethane; at 20 ℃; for 1h;

DOI:10.1021/jo702286b

upstream raw materials:

N-tert-butoxycarbonyl-L-phenylalanine

Downstream raw materials:

1,1-dimethylethyl (S)-1-[(S)-7-(1,1-dimethylethan-1-ylamino)-2-methyl-4,7-dioxoheptan-3-ylamino]-1-oxo-3-phenylpropan-2-ylcarbamate

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