4-nitrophenyl β-D-fucopyranosyl-(1→4)-β-D-2-acetamido-2-deoxy-glucopyranoside

Base Information

Chemical Name:4-nitrophenyl β-D-fucopyranosyl-(1→4)-β-D-2-acetamido-2-deoxy-glucopyranoside
CAS No.:1433713-41-7
Molecular Formula:C₂₀H₂₈N₂O₁₂
Molecular Weight:488.449
Hs Code.:

Synonyms:4-nitrophenyl β-D-fucopyranosyl-(1→4)-β-D-2-acetamido-2-deoxy-glucopyranoside

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Chemical Property of 4-nitrophenyl β-D-fucopyranosyl-(1→4)-β-D-2-acetamido-2-deoxy-glucopyranoside

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Technology Process of 4-nitrophenyl β-D-fucopyranosyl-(1→4)-β-D-2-acetamido-2-deoxy-glucopyranoside

There total 6 articles about 4-nitrophenyl β-D-fucopyranosyl-(1→4)-β-D-2-acetamido-2-deoxy-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 1007855-15-3
α-D-fucopyranosyl fluoride

: 3459-18-5,50645-66-4
4-nitrophenyl N-acetyl-β-D-glucosaminide

: 1433713-41-7,259143-52-7
4-nitrophenyl β-D-fucopyranosyl-(1→4)-β-D-2-acetamido-2-deoxy-glucopyranoside

Guidance literature:: With Thermus nonproteolyticus HG₁₀₂ E₃₃₈A mutant; glycine; sodium hydroxide; In N,N-dimethyl-formamide; at 45 ℃; for 48h; pH=8.8; Enzymatic reaction;
DOI:10.1002/ejoc.201201507

Reference yield:

: 1220893-04-8
2,3,4-tri-O-acetyl-α-D-fucopyranosyl fluoride

: 1433713-41-7,259143-52-7
4-nitrophenyl β-D-fucopyranosyl-(1→4)-β-D-2-acetamido-2-deoxy-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; sodium methylate / 20 °C

2: sodium hydroxide; Thermus nonproteolyticus HG₁₀₂ E₃₃₈A mutant; glycine / N,N-dimethyl-formamide / 48 h / 45 °C / pH 8.8 / Enzymatic reaction

With methanol; Thermus nonproteolyticus HG₁₀₂ E₃₃₈A mutant; sodium methylate; glycine; sodium hydroxide; In N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201201507

Reference yield:

: 51921-33-6
1,2,3,4-tetra-O-acetyl-D-fucopyranose

: 1433713-41-7,259143-52-7
4-nitrophenyl β-D-fucopyranosyl-(1→4)-β-D-2-acetamido-2-deoxy-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; hydrogen fluoride / -20 - 20 °C

2: methanol; sodium methylate / 20 °C

3: sodium hydroxide; Thermus nonproteolyticus HG₁₀₂ E₃₃₈A mutant; glycine / N,N-dimethyl-formamide / 48 h / 45 °C / pH 8.8 / Enzymatic reaction

With pyridine; methanol; Thermus nonproteolyticus HG₁₀₂ E₃₃₈A mutant; hydrogen fluoride; sodium methylate; glycine; sodium hydroxide; In N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201201507