3,3'-[methylenebis(1,4-phenylene)]bis(1,5,3-dithiazocinane)

Base Information

• Chemical Name: 3,3'-[methylenebis(1,4-phenylene)]bis(1,5,3-dithiazocinane)
• CAS No.: 1415327-85-3
• Molecular Formula: C₂₃H₃₀N₂S₄
• Molecular Weight: 462.769
• Mol file: 1415327-85-3.mol

Synonyms:3,3'-[methylenebis(1,4-phenylene)]bis(1,5,3-dithiazocinane)

Chemical Property of 3,3'-[methylenebis(1,4-phenylene)]bis(1,5,3-dithiazocinane)

Chemical Property:

Purity/Quality:

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Technology Process of 3,3'-[methylenebis(1,4-phenylene)]bis(1,5,3-dithiazocinane)

There total 2 articles about 3,3'-[methylenebis(1,4-phenylene)]bis(1,5,3-dithiazocinane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

1-oxa-3,7-dithiacyclooctane (1415327-80-8) + 4,4'-diamino diphenyl methane (101-77-9) → 3,3'-[methylenebis(1,4-phenylene)]bis(1,5,3-dithiazocinane) (1415327-85-3)

Guidance literature:

1-oxa-3,7-dithiacyclooctane; With samarium(III) nitrate hexahydrate; In chloroform; at 20 ℃; for 0.5h; Schlenk technique;

4,4'-diamino diphenyl methane; at 20 ℃; for 3h; Schlenk technique;

DOI:10.1007/s10593-012-1098-8

Reference yield: 65.0%

N1,N1,N7,N7-tetramethyl-2,5-dithiaheptane-1,7-diamine (1369273-05-1) + 4,4'-diamino diphenyl methane (101-77-9) → 3,3'-[methylenebis(1,4-phenylene)]bis(1,5,3-dithiazocinane) (1415327-85-3)

Guidance literature:

N¹,N¹,N⁷,N⁷-tetramethyl-2,5-dithiaheptane-1,7-diamine; With samarium(III) nitrate hexahydrate; In chloroform; at 20 ℃; for 0.5h;

4,4'-diamino diphenyl methane; In ethanol; chloroform; at 20 ℃; for 3h;

DOI:10.1134/S107042802003029X

upstream raw materials:

1-oxa-3,7-dithiacyclooctane

4,4'-diamino diphenyl methane

N¹,N¹,N⁷,N⁷-tetramethyl-2,5-dithiaheptane-1,7-diamine