bis(ethoxycarbonylmethyl) 1,4-dihydro-2,6-dimethyl-4-(3'-nitrophenyl)pyridine-3,5-dicarboxylate

Base Information

Chemical Name:bis(ethoxycarbonylmethyl) 1,4-dihydro-2,6-dimethyl-4-(3'-nitrophenyl)pyridine-3,5-dicarboxylate
CAS No.:152253-22-0
Molecular Formula:C₂₃H₂₆N₂O₁₀
Molecular Weight:490.467
Hs Code.:

Synonyms:bis(ethoxycarbonylmethyl) 1,4-dihydro-2,6-dimethyl-4-(3'-nitrophenyl)pyridine-3,5-dicarboxylate

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Chemical Property of bis(ethoxycarbonylmethyl) 1,4-dihydro-2,6-dimethyl-4-(3'-nitrophenyl)pyridine-3,5-dicarboxylate

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Technology Process of bis(ethoxycarbonylmethyl) 1,4-dihydro-2,6-dimethyl-4-(3'-nitrophenyl)pyridine-3,5-dicarboxylate

There total 1 articles about bis(ethoxycarbonylmethyl) 1,4-dihydro-2,6-dimethyl-4-(3'-nitrophenyl)pyridine-3,5-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 99-61-6
3-nitro-benzaldehyde

: 57582-45-3
ethoxycarbonylmethyl acetoacetate

: 152253-22-0
bis(ethoxycarbonylmethyl) 1,4-dihydro-2,6-dimethyl-4-(3'-nitrophenyl)pyridine-3,5-dicarboxylate

Guidance literature:: With ammonium hydroxide; In ethanol; for 6h; Heating;
DOI:10.1016/S0957-4166(00)00441-9

Reference yield: 60.0%

: 152253-22-0
bis(ethoxycarbonylmethyl) 1,4-dihydro-2,6-dimethyl-4-(3'-nitrophenyl)pyridine-3,5-dicarboxylate

: (R)-2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid monoethoxycarbonylmethyl ester

Guidance literature:: In dimethyl sulfoxide; for 72h; Ambient temperature; seaprose S_. (Aspergillus mellens), phosphate buffer pH 7.8;
DOI:10.1016/S0040-4039(00)79178-7

Reference yield: 29.0%

: 152253-22-0
bis(ethoxycarbonylmethyl) 1,4-dihydro-2,6-dimethyl-4-(3'-nitrophenyl)pyridine-3,5-dicarboxylate

: (R)-2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid monoethoxycarbonylmethyl ester

: (S)-2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid monoethoxycarbonylmethyl ester

Guidance literature:: With water; In di-isopropyl ether; at 20 ℃; for 17h; Product distribution; mutants of lipase PS catalyzed hydrolysis;
DOI:10.1016/0040-4039(94)02454-J