N¹-(4-(sec-butyl)phenyl)-N²-(pyridin-2-ylmethyl)diazene-1,2-dicarboxamide

Base Information

Chemical Name:N¹-(4-(sec-butyl)phenyl)-N²-(pyridin-2-ylmethyl)diazene-1,2-dicarboxamide
CAS No.:1563536-51-5
Molecular Formula:C₁₈H₂₁N₅O₂
Molecular Weight:339.397
Hs Code.:

N<SUP>1</SUP>-(4-(sec-butyl)phenyl)-N<SUP>2</SUP>-(pyridin-2-ylmethyl)diazene-1,2-dicarboxamide

Synonyms:N¹-(4-(sec-butyl)phenyl)-N²-(pyridin-2-ylmethyl)diazene-1,2-dicarboxamide

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Chemical Property of N¹-(4-(sec-butyl)phenyl)-N²-(pyridin-2-ylmethyl)diazene-1,2-dicarboxamide

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Technology Process of N¹-(4-(sec-butyl)phenyl)-N²-(pyridin-2-ylmethyl)diazene-1,2-dicarboxamide

There total 3 articles about N¹-(4-(sec-butyl)phenyl)-N²-(pyridin-2-ylmethyl)diazene-1,2-dicarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 3731-51-9
2-(Aminomethyl)pyridine

: 1563536-45-7
ethyl 2-((4-(sec-butyl)phenyl)carbamoyl)diazenecarboxylate

: 1563536-51-5
N¹-(4-(sec-butyl)phenyl)-N²-(pyridin-2-ylmethyl)diazene-1,2-dicarboxamide

Guidance literature:: In methanol; at -15 - 20 ℃; for 21h;

Reference yield:

: 480439-26-7
4-sec-butylphenyl isocyanate

: 1563536-51-5
N¹-(4-(sec-butyl)phenyl)-N²-(pyridin-2-ylmethyl)diazene-1,2-dicarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: 0.5 h / 0 - 20 °C

2: pyridine; N-Bromosuccinimide / dichloromethane / 1 h / 20 °C

3: methanol / 21 h / -15 - 20 °C

With pyridine; N-Bromosuccinimide; In methanol; dichloromethane;

Reference yield:

: 900085-87-2
ethyl 2-((4-(sec-butyl)phenyl)carbamoyl)hydrazinecarboxylate

: 1563536-51-5
N¹-(4-(sec-butyl)phenyl)-N²-(pyridin-2-ylmethyl)diazene-1,2-dicarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; N-Bromosuccinimide / dichloromethane / 1 h / 20 °C

2: methanol / 21 h / -15 - 20 °C

With pyridine; N-Bromosuccinimide; In methanol; dichloromethane;