Technology Process of C24H31F3O8S
There total 10 articles about C24H31F3O8S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
lithium hexamethyldisilazane;
In
tetrahydrofuran;
at -78 - 20 ℃;
for 0.333333h;
Inert atmosphere;
DOI:10.1002/anie.201103270
- Guidance literature:
-
Multi-step reaction with 3 steps
1: n-butyllithium / tetrahydrofuran; hexane / 0.42 h / -78 - 0 °C / Inert atmosphere
2: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 3 h / 110 °C / Inert atmosphere
3: lithium hexamethyldisilazane / tetrahydrofuran / 0.33 h / -78 - 20 °C / Inert atmosphere
With
n-butyllithium; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; lithium hexamethyldisilazane;
In
tetrahydrofuran; hexane; toluene;
DOI:10.1002/anie.201103270
- Guidance literature:
-
Multi-step reaction with 5 steps
1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 0 - 20 °C / Inert atmosphere
2: camphor-10-sulfonic acid / dichloromethane / 14 h / 0 - 20 °C / Inert atmosphere
3: n-butyllithium / tetrahydrofuran; hexane / 0.42 h / -78 - 0 °C / Inert atmosphere
4: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 3 h / 110 °C / Inert atmosphere
5: lithium hexamethyldisilazane / tetrahydrofuran / 0.33 h / -78 - 20 °C / Inert atmosphere
With
n-butyllithium; 2,2'-azobis(isobutyronitrile); camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; tri-n-butyl-tin hydride; lithium hexamethyldisilazane;
In
tetrahydrofuran; hexane; dichloromethane; toluene;
DOI:10.1002/anie.201103270