17-(2-methoxy-6-phenyl-pyrimidin-4-yloxy)-13-methyl-2,14-dioxo-3,13,15-triaza-tricyclo[13.3.0.04,6]octadec-7-ene-4-carboxylic acid ethyl ester

Base Information

Chemical Name:17-(2-methoxy-6-phenyl-pyrimidin-4-yloxy)-13-methyl-2,14-dioxo-3,13,15-triaza-tricyclo[13.3.0.0*4,6*]octadec-7-ene-4-carboxylic acid ethyl ester
CAS No.:1044559-23-0
Molecular Formula:C₃₀H₃₇N₅O₆
Molecular Weight:563.654
Hs Code.:

Synonyms:17-(2-methoxy-6-phenyl-pyrimidin-4-yloxy)-13-methyl-2,14-dioxo-3,13,15-triaza-tricyclo[13.3.0.0*4,6*]octadec-7-ene-4-carboxylic acid ethyl ester

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Chemical Property of 17-(2-methoxy-6-phenyl-pyrimidin-4-yloxy)-13-methyl-2,14-dioxo-3,13,15-triaza-tricyclo[13.3.0.0*4,6*]octadec-7-ene-4-carboxylic acid ethyl ester

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Technology Process of 17-(2-methoxy-6-phenyl-pyrimidin-4-yloxy)-13-methyl-2,14-dioxo-3,13,15-triaza-tricyclo[13.3.0.0*4,6*]octadec-7-ene-4-carboxylic acid ethyl ester

There total 1 articles about 17-(2-methoxy-6-phenyl-pyrimidin-4-yloxy)-13-methyl-2,14-dioxo-3,13,15-triaza-tricyclo[13.3.0.0*4,6*]octadec-7-ene-4-carboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1044559-21-8
2-methoxy-6-phenylpyrimidin-4-ol

: 922726-54-3
17-hydroxy-13-methyl-2,14-dioxo-3,13,15-triaza-tricyclo[13.3.0.0*4.6*]-octadec-7-ene-4-carboxylic acid ethyl ester

: 603-35-0
triphenylphosphine

: 1044559-23-0
17-(2-methoxy-6-phenyl-pyrimidin-4-yloxy)-13-methyl-2,14-dioxo-3,13,15-triaza-tricyclo[13.3.0.0*4,6*]octadec-7-ene-4-carboxylic acid ethyl ester

: 791-28-6
Triphenylphosphine oxide

Guidance literature:: With di-isopropyl azodicarboxylate; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 - 20 ℃;

Reference yield: 86.0%

: 1044559-23-0
17-(2-methoxy-6-phenyl-pyrimidin-4-yloxy)-13-methyl-2,14-dioxo-3,13,15-triaza-tricyclo[13.3.0.0*4,6*]octadec-7-ene-4-carboxylic acid ethyl ester

: 1044559-25-2
17-(2-methoxy-6-phenyl-pyrimidin-4-yloxy)-13-methyl-2,14-dioxo-3,13,15-triaza-tricyclo[13.3.0.0*4,6*]octadec-7-ene-4-carboxylic acid

Guidance literature:: 17-(2-methoxy-6-phenyl-pyrimidin-4-yloxy)-13-methyl-2,14-dioxo-3,13,15-triaza-tricyclo[13.3.0.0*4,6*]octadec-7-ene-4-carboxylic acid ethyl ester; With methanol; lithium hydroxide; water; In tetrahydrofuran; at 20 ℃;

With citric acid; In tetrahydrofuran; methanol; water;

Reference yield:

: 1044559-23-0
17-(2-methoxy-6-phenyl-pyrimidin-4-yloxy)-13-methyl-2,14-dioxo-3,13,15-triaza-tricyclo[13.3.0.0*4,6*]octadec-7-ene-4-carboxylic acid ethyl ester

: 1044558-56-6
cyclopropanesulfonic acid [17-(2-methoxy-6-phenyl-pyrimidin-4-yloxy)-13-methyl-2,14-dioxo-3,13,15-triaza-tricyclo[13.3.0.0*4,6*]octadec-7-ene-4-carbonyl]-amide

Guidance literature:: Multi-step reaction with 2 steps

1.1: methanol; lithium hydroxide; water / tetrahydrofuran / 20 °C

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / 20 °C

2.2: 3.5 h / 20 °C

With methanol; lithium hydroxide; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; dichloromethane;