N-trifluoroacetyl-2-(2,5-dimethoxy-4-(phenylacetyl)-phenyl)-1-aminoethane

Base Information

Chemical Name:N-trifluoroacetyl-2-(2,5-dimethoxy-4-(phenylacetyl)-phenyl)-1-aminoethane
CAS No.:289889-64-1
Molecular Formula:C₂₀H₂₀F₃NO₄
Molecular Weight:395.378
Hs Code.:

Synonyms:N-trifluoroacetyl-2-(2,5-dimethoxy-4-(phenylacetyl)-phenyl)-1-aminoethane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-trifluoroacetyl-2-(2,5-dimethoxy-4-(phenylacetyl)-phenyl)-1-aminoethane

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Technology Process of N-trifluoroacetyl-2-(2,5-dimethoxy-4-(phenylacetyl)-phenyl)-1-aminoethane

There total 2 articles about N-trifluoroacetyl-2-(2,5-dimethoxy-4-(phenylacetyl)-phenyl)-1-aminoethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 501-53-1,94274-21-2
benzyl chloroformate

: 187389-19-1
N-trifluoroacetyl-2-(2,5-dimethoxyphenyl)-1-aminoethane

: 289889-64-1
N-trifluoroacetyl-2-(2,5-dimethoxy-4-(phenylacetyl)-phenyl)-1-aminoethane

Guidance literature:: With titanium tetrachloride; In dichloromethane; at -30 - 20 ℃;
DOI:10.1021/jm9906062

Reference yield:

: 3600-86-0
2,5-dimethoxyphenethylamine

: 289889-64-1
N-trifluoroacetyl-2-(2,5-dimethoxy-4-(phenylacetyl)-phenyl)-1-aminoethane

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / 0 °C

2: 18 percent / TiCl₄ / CH₂Cl₂ / -30 - 20 °C

With titanium tetrachloride; In dichloromethane; 1: Acetylation / 2: Friedel-Crafts acylation;
DOI:10.1021/jm9906062

Reference yield: 79.0%

: 289889-64-1
N-trifluoroacetyl-2-(2,5-dimethoxy-4-(phenylacetyl)-phenyl)-1-aminoethane

: 289889-68-5
N-trifluoroacetyl-2-[2,5-dimethoxy-4-(2-phenylethyl)phenyl]-1-amionoethane

Guidance literature:: With perchloric acid; hydrogen; acetic acid; palladium on activated charcoal; for 6h; under 3102.89 Torr;
DOI:10.1021/jm9906062