C₂₅H₃₂N₂O₃

Base Information

Chemical Name:C₂₅H₃₂N₂O₃
CAS No.:1616108-01-0
Molecular Formula:C₂₅H₃₂N₂O₃
Molecular Weight:408.541
Hs Code.:

C<sub>25</sub>H<sub>32</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:C₂₅H₃₂N₂O₃

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Chemical Property of C₂₅H₃₂N₂O₃

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Technology Process of C₂₅H₃₂N₂O₃

There total 9 articles about C₂₅H₃₂N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 15790-87-1,15790-88-2,818-59-7
methyl 2-pentenoate

: C₁₉H₂₂N₂O

: 1616108-01-0
C₂₅H₃₂N₂O₃

Guidance literature:: C₁₉H₂₂N₂O; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 1h;

methyl 2-pentenoate; In tetrahydrofuran; at -78 ℃; for 2h;
DOI:10.1016/j.tet.2014.05.049

Reference yield:

: 1616107-81-3
(S)-2-amino-3-methoxymethyltetrahydroisoquinoline

: 1616108-01-0
C₂₅H₃₂N₂O₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid / toluene / 0 - 20 °C

2.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C

2.2: 2 h / -78 °C

With n-butyllithium; acetic acid; In tetrahydrofuran; toluene; 2.2: |Michael Addition;
DOI:10.1016/j.tet.2014.05.049

Reference yield:

: 3618-96-0
(S)-N-acetylphenylalanine

: 1616108-01-0
C₂₅H₃₂N₂O₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: lithium borohydride / tetrahydrofuran / 4 h / 0 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 °C

3.1: hydrogenchloride / water / 24 h / Reflux

4.1: formic acid / 20 h / 60 °C

5.1: sodium nitrite; hydrogenchloride / water / 1 h

6.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C

7.1: acetic acid / toluene / 0 - 20 °C

8.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C

8.2: 2 h / -78 °C

With hydrogenchloride; lithium aluminium tetrahydride; lithium borohydride; n-butyllithium; formic acid; sodium hydride; acetic acid; sodium nitrite; In tetrahydrofuran; water; toluene; mineral oil; 8.2: |Michael Addition;
DOI:10.1016/j.tet.2014.05.049