2-chloro-N-<(5,6-dichloro-2-methoxy-3,4-dimethylphenyl)methyl>acetamide

Base Information

• Chemical Name: 2-chloro-N-<(5,6-dichloro-2-methoxy-3,4-dimethylphenyl)methyl>acetamide
• CAS No.: 52780-52-6
• Molecular Formula: C₁₂H₁₄Cl₃NO₂
• Molecular Weight: 310.608

Synonyms:2-chloro-N-<(5,6-dichloro-2-methoxy-3,4-dimethylphenyl)methyl>acetamide

Chemical Property of 2-chloro-N-<(5,6-dichloro-2-methoxy-3,4-dimethylphenyl)methyl>acetamide

Chemical Property:

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Technology Process of 2-chloro-N-<(5,6-dichloro-2-methoxy-3,4-dimethylphenyl)methyl>acetamide

There total 3 articles about 2-chloro-N-<(5,6-dichloro-2-methoxy-3,4-dimethylphenyl)methyl>acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

2-chloro-N-<(5-chloro-2-methoxy-3,4-dimethylphenyl)methyl>acetamide → 2-chloro-N-<(5,6-dichloro-2-methoxy-3,4-dimethylphenyl)methyl>acetamide (52780-52-6)

Guidance literature:

With aluminium trichloride; sulfuryl dichloride; sulfur monochloride; at 80 - 85 ℃; for 1.5h;

DOI:10.1021/jm00186a024

Reference yield:

4-chloro-2,3-dimethylanisole (14804-26-3) → 2-chloro-N-<(5,6-dichloro-2-methoxy-3,4-dimethylphenyl)methyl>acetamide (52780-52-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 81 percent / HOAc, conc. H₂SO₄ / 16 h

2: 24 percent / aluminum chloride, sulfuryl chloride, sulfur monochloride / 1.5 h / 80 - 85 °C

With aluminium trichloride; sulfuryl dichloride; sulfur monochloride; sulfuric acid; acetic acid;

DOI:10.1021/jm00186a024

Reference yield:

→ 2-chloro-N-<(5,6-dichloro-2-methoxy-3,4-dimethylphenyl)methyl>acetamide (52780-52-6)

Guidance literature:

entspr. 6-H-Benzylacetamid, Aluminiumchlorid, Sulfurylchlorid, Schwefelmonochlorid;

upstream raw materials:

4-chloro-2,3-dimethylanisole

Downstream raw materials:

2-(aminomethyl)-3,4-dichloro-5,6-dimethylphenol hydrobromide

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