C₂₀H₂₄O₅

Base Information

Chemical Name:C₂₀H₂₄O₅
CAS No.:1449419-25-3
Molecular Formula:C₂₀H₂₄O₅
Molecular Weight:344.408
Hs Code.:

C<sub>20</sub>H<sub>24</sub>O<sub>5</sub>

Synonyms:C₂₀H₂₄O₅

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Chemical Property of C₂₀H₂₄O₅

Chemical Property:

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Technology Process of C₂₀H₂₄O₅

There total 7 articles about C₂₀H₂₄O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1449419-23-1
C₂₀H₂₄O₄

: 1449419-25-3
C₂₀H₂₄O₅

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; In tetrahydrofuran; water; tert-butyl alcohol; at 4 ℃; for 0.5h;
DOI:10.1016/j.tet.2013.02.008

Reference yield:

: 1449419-17-3
C₁₅H₂₀O₃S₂

: 1449419-25-3
C₂₀H₂₄O₅

Guidance literature:: Multi-step reaction with 7 steps

1.1: diisobutylaluminium hydride / dichloromethane; toluene / 2 h / -78 °C

1.2: 2.5 h / 0 - 20 °C

2.1: magnesium bromide ethyl etherate / dichloromethane / 1 h / -78 °C

2.2: 1.5 h / -78 °C

3.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran; toluene / 21 h / 0 - 20 °C

4.1: sodium hydroxide / tetrahydrofuran; water; methanol / 12 h / 0 - 20 °C

5.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C

5.2: 21.5 h / 0 - 20 °C

6.1: sodium hydrogencarbonate; methyl iodide / acetonitrile; water / 19 h / 20 °C

7.1: sodium dihydrogenphosphate; 2-methyl-but-2-ene; sodium chlorite / tetrahydrofuran; water; tert-butyl alcohol / 0.5 h / 4 °C

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; di-isopropyl azodicarboxylate; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; magnesium bromide ethyl etherate; triphenylphosphine; sodium hydroxide; methyl iodide; In tetrahydrofuran; methanol; dichloromethane; water; toluene; acetonitrile; mineral oil; tert-butyl alcohol; 2.2: |Grignard Reaction / 3.1: |Mitsunobu Displacement;
DOI:10.1016/j.tet.2013.02.008

Reference yield:

: 1449419-19-5
C₁₆H₂₄O₃S₂

: 1449419-25-3
C₂₀H₂₄O₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran; toluene / 21 h / 0 - 20 °C

2.1: sodium hydroxide / tetrahydrofuran; water; methanol / 12 h / 0 - 20 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C

3.2: 21.5 h / 0 - 20 °C

4.1: sodium hydrogencarbonate; methyl iodide / acetonitrile; water / 19 h / 20 °C

5.1: sodium dihydrogenphosphate; 2-methyl-but-2-ene; sodium chlorite / tetrahydrofuran; water; tert-butyl alcohol / 0.5 h / 4 °C

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; di-isopropyl azodicarboxylate; sodium hydride; sodium hydrogencarbonate; triphenylphosphine; sodium hydroxide; methyl iodide; In tetrahydrofuran; methanol; water; toluene; acetonitrile; mineral oil; tert-butyl alcohol; 1.1: |Mitsunobu Displacement;
DOI:10.1016/j.tet.2013.02.008