C₁₀₃H₁₁₂N₄O₂₂

Base Information

• Chemical Name: C₁₀₃H₁₁₂N₄O₂₂
• CAS No.: 1400594-82-2
• Molecular Formula: C₁₀₃H₁₁₂N₄O₂₂
• Molecular Weight: 1758.04

Synonyms:C₁₀₃H₁₁₂N₄O₂₂

Chemical Property of C₁₀₃H₁₁₂N₄O₂₂

Chemical Property:

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Technology Process of C₁₀₃H₁₁₂N₄O₂₂

There total 1 articles about C₁₀₃H₁₁₂N₄O₂₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

N-benzyl-N-benzyloxycarbonyl-5-aminopentyl O-[2-azido-6-O-benzyl-2-deoxy-4-O-(9-fluorenylmethyloxycarbonyl)-3-O-(2-methylnaphthyl)-α-D-glucopyranosyl]-(1→4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-mannopyranosyl)-(1→4)-6-O-benzyl-2-deoxy-3-O-levulinoyl-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside (1400594-81-1) + acetic anhydride (108-24-7) → C103H112N4O22 (1400594-82-2)

Guidance literature:

With water; copper(II) sulfate; acetic acid; zinc; In tetrahydrofuran; at 20 ℃; for 0.75h;

DOI:10.1021/ja3069962

Reference yield:

C103H112N4O22 (1400594-82-2) → C88H100N4O20

Guidance literature:

With methanol; sodium methylate; In dichloromethane; at 20 ℃; for 12h;

DOI:10.1021/ja3069962

upstream raw materials:

N-benzyl-N-benzyloxycarbonyl-5-aminopentyl O-[2-azido-6-O-benzyl-2-deoxy-4-O-(9-fluorenylmethyloxycarbonyl)-3-O-(2-methylnaphthyl)-α-D-glucopyranosyl]-(1→4)-O-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-mannopyranosyl)-(1→4)-6-O-benzyl-2-deoxy-3-O-levulinoyl-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

acetic anhydride

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