C₄₇H₅₁F₂N₇O₇

Base Information

Chemical Name:C₄₇H₅₁F₂N₇O₇
CAS No.:1369595-61-8
Molecular Formula:C₄₇H₅₁F₂N₇O₇
Molecular Weight:863.961
Hs Code.:

C<sub>47</sub>H<sub>51</sub>F<sub>2</sub>N<sub>7</sub>O<sub>7</sub>

Synonyms:C₄₇H₅₁F₂N₇O₇

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₇H₅₁F₂N₇O₇

Chemical Property:

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Technology Process of C₄₇H₅₁F₂N₇O₇

There total 12 articles about C₄₇H₅₁F₂N₇O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1369594-33-1
tert-butyl (2S,4R)-2-(5-bromo-1H-imidazol-2-yl)-4-fluoropyrrolidine-1-carboxylate

: 1369595-44-7
C₃₅H₄₁B₂NO₇

: 1369595-61-8
C₄₇H₅₁F₂N₇O₇

Guidance literature:: With potassium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; water; at 90 ℃; for 18h; Inert atmosphere;

Reference yield:

: 30186-18-6
4'-bromo-2'-hydroxyacetophenone

: 1369595-61-8
C₄₇H₅₁F₂N₇O₇

Guidance literature:: Multi-step reaction with 5 steps

1: acetic acid / ethanol / 6 h / Reflux

2: polyphosphoric acid / 2 h / 80 °C

3: caesium carbonate / dimethyl sulfoxide / 18 h / 90 °C

4: potassium acetate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 0.75 h / 90 °C / Inert atmosphere; Microwave irradiation

5: potassium carbonate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane; water / 18 h / 90 °C / Inert atmosphere

With potassium acetate; potassium carbonate; caesium carbonate; acetic acid; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; ethanol; water; dimethyl sulfoxide;

Reference yield:

: 203866-14-2
(2S,4R)-1-[(tert-butoxy)carbonyl]-4-fluoropyrrolidine-2-carboxylic acid

: 1369595-61-8
C₄₇H₅₁F₂N₇O₇

Guidance literature:: Multi-step reaction with 6 steps

1.1: borane-THF / tetrahydrofuran / 15 h / 0 - 20 °C

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C

2.2: 1.5 h / -78 - 0 °C

3.1: ammonia / methanol / 39 h / 20 °C

4.1: N-Bromosuccinimide / acetonitrile / 15 h / 20 °C

5.1: sodium sulfite / ethanol; water / 39 h / Reflux

6.1: potassium carbonate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane; water / 18 h / 90 °C / Inert atmosphere

With N-Bromosuccinimide; borane-THF; oxalyl dichloride; ammonia; potassium carbonate; dimethyl sulfoxide; sodium sulfite; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; water; acetonitrile;