benzyloxycarbonyl 2-N-(benzyloxycarbonyl)-2-deoxy-2-methylamino-4:6-ethylidene-L-glucopyranoside

Base Information

Chemical Name:benzyloxycarbonyl 2-N-(benzyloxycarbonyl)-2-deoxy-2-methylamino-4:6-ethylidene-L-glucopyranoside
CAS No.:111275-62-8
Molecular Formula:C₂₅H₂₉NO₉
Molecular Weight:487.507
Hs Code.:

Synonyms:benzyloxycarbonyl 2-N-(benzyloxycarbonyl)-2-deoxy-2-methylamino-4:6-ethylidene-L-glucopyranoside

Suppliers and Price of benzyloxycarbonyl 2-N-(benzyloxycarbonyl)-2-deoxy-2-methylamino-4:6-ethylidene-L-glucopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of benzyloxycarbonyl 2-N-(benzyloxycarbonyl)-2-deoxy-2-methylamino-4:6-ethylidene-L-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of benzyloxycarbonyl 2-N-(benzyloxycarbonyl)-2-deoxy-2-methylamino-4:6-ethylidene-L-glucopyranoside

There total 4 articles about benzyloxycarbonyl 2-N-(benzyloxycarbonyl)-2-deoxy-2-methylamino-4:6-ethylidene-L-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 501-53-1,94274-21-2
benzyl chloroformate

: 2-N-(benzyloxycarbonyl)-2-deoxy-2-methylamino-4:6-ethylidene-L-glucopyranose

: 111275-62-8
benzyloxycarbonyl 2-N-(benzyloxycarbonyl)-2-deoxy-2-methylamino-4:6-ethylidene-L-glucopyranoside

Guidance literature:: With sodium hydroxide; In 1,4-dioxane; water; for 0.5h; Ambient temperature;
DOI:10.1248/cpb.34.3733

Reference yield:

: 7474-39-7,18378-96-6,23846-26-6,33423-05-1,33423-23-3
2-deoxy-2-methylamino-L-glucopyranose hydrochloride

: 111275-62-8
benzyloxycarbonyl 2-N-(benzyloxycarbonyl)-2-deoxy-2-methylamino-4:6-ethylidene-L-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / sodium carbonate / H₂O; acetone / 1 h / 0 °C

2: 60 percent / conc. sulfuric acid / 3 h / Ambient temperature

3: 43 percent / 30percent sodium hydroxide / H₂O; dioxane / 0.5 h / Ambient temperature

With sodium hydroxide; sulfuric acid; sodium carbonate; In 1,4-dioxane; water; acetone;
DOI:10.1248/cpb.34.3733

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 111275-62-8
benzyloxycarbonyl 2-N-(benzyloxycarbonyl)-2-deoxy-2-methylamino-4:6-ethylidene-L-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / sodium carbonate / H₂O; acetone / 1 h / 0 °C

2: 60 percent / conc. sulfuric acid / 3 h / Ambient temperature

3: 43 percent / 30percent sodium hydroxide / H₂O; dioxane / 0.5 h / Ambient temperature

With sodium hydroxide; sulfuric acid; sodium carbonate; In 1,4-dioxane; water; acetone;
DOI:10.1248/cpb.34.3733