1-Benzyl-3-(4-methoxy-3-methyl-benzyl)-6-[1-(2,4,5-trimethoxy-3-methyl-phenyl)-meth-(Z)-ylidene]-piperazine-2,5-dione

Base Information

Chemical Name:1-Benzyl-3-(4-methoxy-3-methyl-benzyl)-6-[1-(2,4,5-trimethoxy-3-methyl-phenyl)-meth-(Z)-ylidene]-piperazine-2,5-dione
CAS No.:168132-72-7
Molecular Formula:C₃₁H₃₄N₂O₆
Molecular Weight:530.621
Hs Code.:

Synonyms:1-Benzyl-3-(4-methoxy-3-methyl-benzyl)-6-[1-(2,4,5-trimethoxy-3-methyl-phenyl)-meth-(Z)-ylidene]-piperazine-2,5-dione

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Chemical Property of 1-Benzyl-3-(4-methoxy-3-methyl-benzyl)-6-[1-(2,4,5-trimethoxy-3-methyl-phenyl)-meth-(Z)-ylidene]-piperazine-2,5-dione

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Technology Process of 1-Benzyl-3-(4-methoxy-3-methyl-benzyl)-6-[1-(2,4,5-trimethoxy-3-methyl-phenyl)-meth-(Z)-ylidene]-piperazine-2,5-dione

There total 3 articles about 1-Benzyl-3-(4-methoxy-3-methyl-benzyl)-6-[1-(2,4,5-trimethoxy-3-methyl-phenyl)-meth-(Z)-ylidene]-piperazine-2,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1-Acetyl-4-benzyl-6-(4-methoxy-3-methyl-benzyl)-3-[1-(2,4,5-trimethoxy-3-methyl-phenyl)-meth-(Z)-ylidene]-piperazine-2,5-dione

: 168132-72-7
1-Benzyl-3-(4-methoxy-3-methyl-benzyl)-6-[1-(2,4,5-trimethoxy-3-methyl-phenyl)-meth-(Z)-ylidene]-piperazine-2,5-dione

Guidance literature:: With hydrazine hydrate; In N,N-dimethyl-formamide; for 1h; Ambient temperature;
DOI:10.1016/0040-4020(95)00437-D

Reference yield:

: 168132-73-8
(Z)-1-<(isopropyloxy)carbonyl>-4-benzyl-6-(4-methoxy-3-methylphenylmethyl)-3-(2,4,5-trimethoxy-3-methylphenylmethylene)-2,5-piperazinedione

: 168132-72-7
1-Benzyl-3-(4-methoxy-3-methyl-benzyl)-6-[1-(2,4,5-trimethoxy-3-methyl-phenyl)-meth-(Z)-ylidene]-piperazine-2,5-dione

: 4-Benzyl-2-hydroxy-6-(4-methoxy-3-methyl-benzyl)-5-oxo-3-[1-(2,4,5-trimethoxy-3-methyl-phenyl)-meth-(Z)-ylidene]-piperazine-1-carboxylic acid isopropyl ester

Guidance literature:: With lithium tri(t-butoxy)aluminum hydride; In tetrahydrofuran; at 0 ℃; for 1h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1016/0040-4020(95)00437-D

Reference yield:

: 168132-73-8
(Z)-1-<(isopropyloxy)carbonyl>-4-benzyl-6-(4-methoxy-3-methylphenylmethyl)-3-(2,4,5-trimethoxy-3-methylphenylmethylene)-2,5-piperazinedione

: 168132-72-7
1-Benzyl-3-(4-methoxy-3-methyl-benzyl)-6-[1-(2,4,5-trimethoxy-3-methyl-phenyl)-meth-(Z)-ylidene]-piperazine-2,5-dione

: (E)-3-benzyl-2-<(1,2,3,4,5,6-hexahydro-2,4,5-trimethoxy-3-methylphenyl)methylene>-9-methoxy-8-methyl-4-oxo-1,5-imino-3-benzazocine-11-carboxylic acid isopropyl ester

: 1-Benzyl-5,6,8-trimethoxy-3-(4-methoxy-3-methyl-benzyl)-7-methyl-2-oxo-1,2,3,9-tetrahydro-indeno[1,2-b]pyrazine-4-carboxylic acid isopropyl ester

Guidance literature:: With lithium tri(t-butoxy)aluminum hydride; boron trifluoride diethyl etherate; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, 0 deg C, 1 h, 2.) CH₂Cl₂, 14 h, RT;
DOI:10.1016/0040-4020(95)00437-D