N-(3,5-ditrifluoromethyl)benzyl-O-⁽⁹⁾-(3,5-ditrifluoro-methylbenzyl)quinidinium bromide

Base Information

• Chemical Name: N-(3,5-ditrifluoromethyl)benzyl-O-⁽⁹⁾-(3,5-ditrifluoro-methylbenzyl)quinidinium bromide
• CAS No.: 1415666-65-7
• Molecular Formula: Br*C₃₈H₃₃F₁₂N₂O₂
• Molecular Weight: 857.577

Synonyms:N-(3,5-ditrifluoromethyl)benzyl-O-⁽⁹⁾-(3,5-ditrifluoro-methylbenzyl)quinidinium bromide

Chemical Property of N-(3,5-ditrifluoromethyl)benzyl-O-⁽⁹⁾-(3,5-ditrifluoro-methylbenzyl)quinidinium bromide

Chemical Property:

Purity/Quality:

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Technology Process of N-(3,5-ditrifluoromethyl)benzyl-O-⁽⁹⁾-(3,5-ditrifluoro-methylbenzyl)quinidinium bromide

There total 3 articles about N-(3,5-ditrifluoromethyl)benzyl-O-⁽⁹⁾-(3,5-ditrifluoro-methylbenzyl)quinidinium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

N-[3,5-bis(trifluoromethyl)benzyl]quinidinium bromide (945732-76-3,1415666-63-5) + 3,5-bis(trifluoromethyl)benzyl bromide (32247-96-4) → N-(3,5-ditrifluoromethyl)benzyl-O-(9)-(3,5-ditrifluoro-methylbenzyl)quinidinium bromide (1415666-65-7)

Guidance literature:

With potassium hydroxide; In dichloromethane; at 20 ℃; for 4h; Inert atmosphere;

DOI:10.1016/j.jfluchem.2013.01.027

Reference yield:

quinidine (56-54-2) → N-(3,5-ditrifluoromethyl)benzyl-O-(9)-(3,5-ditrifluoro-methylbenzyl)quinidinium bromide (1415666-65-7)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene / 80 °C / Inert atmosphere

2: potassium hydroxide / dichloromethane / 4 h / 20 °C / Inert atmosphere

With potassium hydroxide; In dichloromethane; toluene;

DOI:10.1016/j.jfluchem.2013.01.027

Reference yield:

3,5-bis(trifluoromethyl)benzyl bromide (32247-96-4) → N-(3,5-ditrifluoromethyl)benzyl-O-(9)-(3,5-ditrifluoro-methylbenzyl)quinidinium bromide (1415666-65-7)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene / 80 °C / Inert atmosphere

2: potassium hydroxide / dichloromethane / 4 h / 20 °C / Inert atmosphere

With potassium hydroxide; In dichloromethane; toluene;

DOI:10.1016/j.jfluchem.2013.01.027

upstream raw materials:

N-[3,5-bis(trifluoromethyl)benzyl]quinidinium bromide

3,5-bis(trifluoromethyl)benzyl bromide

quinidine

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