but-2-enedioic acid allyl ester 3-(3-allyloxycarbonyl-acryloyloxymethyl)-benzyl ester

Base Information

Chemical Name:but-2-enedioic acid allyl ester 3-(3-allyloxycarbonyl-acryloyloxymethyl)-benzyl ester
CAS No.:929539-00-4
Molecular Formula:C₂₂H₂₂O₈
Molecular Weight:414.412
Hs Code.:

Synonyms:but-2-enedioic acid allyl ester 3-(3-allyloxycarbonyl-acryloyloxymethyl)-benzyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of but-2-enedioic acid allyl ester 3-(3-allyloxycarbonyl-acryloyloxymethyl)-benzyl ester

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Technology Process of but-2-enedioic acid allyl ester 3-(3-allyloxycarbonyl-acryloyloxymethyl)-benzyl ester

There total 2 articles about but-2-enedioic acid allyl ester 3-(3-allyloxycarbonyl-acryloyloxymethyl)-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 929538-92-1
but-2-enedioic acid mono-[3-(3-carboxy-acryloyloxymethyl)-benzyl] ester

: 106-95-6
allyl bromide

: 929539-00-4
but-2-enedioic acid allyl ester 3-(3-allyloxycarbonyl-acryloyloxymethyl)-benzyl ester

Guidance literature:: With tetra-(n-butyl)ammonium iodide; potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 6h;
DOI:10.1021/jo062043p

Reference yield:

: 626-18-6
1,3-dimethanol benzene

: 929539-00-4
but-2-enedioic acid allyl ester 3-(3-allyloxycarbonyl-acryloyloxymethyl)-benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / triethylamine / CH₂Cl₂ / 9 h / 0 - 20 °C

2: 90 percent / anhydrous K₂CO₃; tetrabutylammonium iodide / dimethylformamide / 6 h / 20 °C

With tetra-(n-butyl)ammonium iodide; potassium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo062043p