C₃₅H₃₆N₆O₆S₄

Base Information

Chemical Name:C₃₅H₃₆N₆O₆S₄
CAS No.:1391396-84-1
Molecular Formula:C₃₅H₃₆N₆O₆S₄
Molecular Weight:764.971
Hs Code.:

C<sub>35</sub>H<sub>36</sub>N<sub>6</sub>O<sub>6</sub>S<sub>4</sub>

Synonyms:C₃₅H₃₆N₆O₆S₄

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Chemical Property of C₃₅H₃₆N₆O₆S₄

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Technology Process of C₃₅H₃₆N₆O₆S₄

There total 18 articles about C₃₅H₃₆N₆O₆S₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1391396-68-1
C₁₃H₁₀BrNO₄

: 1391396-64-7
C₂₂H₂₉N₅O₃S₄

: 1391396-84-1
C₃₅H₃₆N₆O₆S₄

Guidance literature:: C₁₃H₁₀BrNO₄; C₂₂H₂₉N₅O₃S₄; With potassium hydrogencarbonate; In 1,2-dimethoxyethane; at 20 ℃; for 16h; Inert atmosphere;

With pyridine; trifluoroacetic anhydride; In 1,2-dimethoxyethane; at 0 ℃; for 3h; Inert atmosphere;

With triethylamine; In 1,2-dimethoxyethane; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.tetlet.2012.05.105

Reference yield:

: C₂₂H₂₉N₅O₄S₃

: 1391396-84-1
C₃₅H₃₆N₆O₆S₄

Guidance literature:: Multi-step reaction with 2 steps

1.1: Lawessons reagent / benzene / 5 h / Inert atmosphere; Reflux

2.1: potassium hydrogencarbonate / 1,2-dimethoxyethane / 16 h / 20 °C / Inert atmosphere

2.2: 3 h / 0 °C / Inert atmosphere

2.3: 3 h / 20 °C / Inert atmosphere

With Lawessons reagent; potassium hydrogencarbonate; In 1,2-dimethoxyethane; benzene; 2.1: Hantzsch thiazole synthesis / 2.2: Hantzsch thiazole synthesis / 2.3: Hantzsch thiazole synthesis;
DOI:10.1016/j.tetlet.2012.05.105

Reference yield:

: Boc-Thr(tBu)-CONH₂

: 1391396-84-1
C₃₅H₃₆N₆O₆S₄

Guidance literature:: Multi-step reaction with 11 steps

1.1: Lawessons reagent / tetrahydrofuran / Inert atmosphere; Reflux

2.1: potassium hydrogencarbonate / 1,2-dimethoxyethane / 16 h / 20 °C / Inert atmosphere

2.2: 3 h / 0 °C / Inert atmosphere

2.3: 3 h / 20 °C / Inert atmosphere

3.1: ammonium hydroxide / methanol; water / 20 °C / Sonication

4.1: Lawessons reagent / 1,2-dimethoxyethane / 5 h / 60 °C / Inert atmosphere

5.1: potassium hydrogencarbonate / 1,2-dimethoxyethane / 16 h / 20 °C / Inert atmosphere

5.2: 3 h / 0 °C / Inert atmosphere

6.1: ammonium hydroxide / methanol; water / 20 °C / Sonication

7.1: Lawessons reagent / benzene / 5 h / 60 °C / Inert atmosphere

8.1: potassium hydrogencarbonate / 1,2-dimethoxyethane / 16 h / 20 °C / Inert atmosphere

8.2: 3 h / 0 °C / Inert atmosphere

9.1: ammonium hydroxide / methanol; water / 20 °C / Sonication

10.1: Lawessons reagent / benzene / 5 h / Inert atmosphere; Reflux

11.1: potassium hydrogencarbonate / 1,2-dimethoxyethane / 16 h / 20 °C / Inert atmosphere

11.2: 3 h / 0 °C / Inert atmosphere

11.3: 3 h / 20 °C / Inert atmosphere

With Lawessons reagent; ammonium hydroxide; potassium hydrogencarbonate; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; water; benzene; 2.1: Hantzsch thiazole synthesis / 2.2: Hantzsch thiazole synthesis / 2.3: Hantzsch thiazole synthesis / 5.1: Hantzsch thiazole synthesis / 5.2: Hantzsch thiazole synthesis / 8.1: Hantzsch thiazole synthesis / 8.2: Hantzsch thiazole synthesis / 11.1: Hantzsch thiazole synthesis / 11.2: Hantzsch thiazole synthesis / 11.3: Hantzsch thiazole synthesis;
DOI:10.1016/j.tetlet.2012.05.105