ethyl 3-(3-benzyloxycarbonylamino-propyl)-5-(3-{4-(3-tert-butoxycarbonylaminopropoxy)-3,5-bis(1,3-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propan-2-yloxy)benzoylamino}propyl)benzoate

Base Information

• Chemical Name: ethyl 3-(3-benzyloxycarbonylamino-propyl)-5-(3-{4-(3-tert-butoxycarbonylaminopropoxy)-3,5-bis(1,3-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propan-2-yloxy)benzoylamino}propyl)benzoate
• CAS No.: 870177-75-6
• Molecular Formula: C₇₂H₁₁₇N₃O₂₆
• Molecular Weight: 1440.73

Synonyms:ethyl 3-(3-benzyloxycarbonylamino-propyl)-5-(3-{4-(3-tert-butoxycarbonylaminopropoxy)-3,5-bis(1,3-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propan-2-yloxy)benzoylamino}propyl)benzoate

Chemical Property of ethyl 3-(3-benzyloxycarbonylamino-propyl)-5-(3-{4-(3-tert-butoxycarbonylaminopropoxy)-3,5-bis(1,3-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propan-2-yloxy)benzoylamino}propyl)benzoate

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Technology Process of ethyl 3-(3-benzyloxycarbonylamino-propyl)-5-(3-{4-(3-tert-butoxycarbonylaminopropoxy)-3,5-bis(1,3-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propan-2-yloxy)benzoylamino}propyl)benzoate

There total 1 articles about ethyl 3-(3-benzyloxycarbonylamino-propyl)-5-(3-{4-(3-tert-butoxycarbonylaminopropoxy)-3,5-bis(1,3-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propan-2-yloxy)benzoylamino}propyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

ethyl 3-[3-(benzyloxycarbonylamino)propyl]-5-(trifluoroacetato-3-ammoniumpropyl)benzoate + 4-(3-tert-butoxycarbonylaminopropoxy)-3,5-bis(1,3-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propan-2-yloxy)benzoic acid (870177-17-6) → ethyl 3-(3-benzyloxycarbonylamino-propyl)-5-(3-{4-(3-tert-butoxycarbonylaminopropoxy)-3,5-bis(1,3-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propan-2-yloxy)benzoylamino}propyl)benzoate (870177-75-6)

Guidance literature:

4-(3-tert-butoxycarbonylaminopropoxy)-3,5-bis(1,3-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propan-2-yloxy)benzoic acid; With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; In dichloromethane; N,N-dimethyl-formamide; at -20 - 20 ℃;

ethyl 3-[3-(benzyloxycarbonylamino)propyl]-5-(trifluoroacetato-3-ammoniumpropyl)benzoate; With triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide; at -40 - 20 ℃;

DOI:10.1002/chem.200401078

Reference yield: 98.0%

ethyl 3-(3-benzyloxycarbonylamino-propyl)-5-(3-{4-(3-tert-butoxycarbonylaminopropoxy)-3,5-bis(1,3-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propan-2-yloxy)benzoylamino}propyl)benzoate (870177-75-6) → 3-(3-benzyloxycarbonylamino-propyl)-5-(3-{4-(3-tert-butoxycarbonylaminopropoxy)-3,5-bis(1,3-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propan-2-yloxy)benzoylamino}propyl)benzoic acid

Guidance literature:

With potassium hydroxide; In ethanol; at 20 ℃; for 12h;

DOI:10.1002/chem.200401078

Reference yield: 89.0%

ethyl 3-(3-benzyloxycarbonylamino-propyl)-5-(3-{4-(3-tert-butoxycarbonylaminopropoxy)-3,5-bis(1,3-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propan-2-yloxy)benzoylamino}propyl)benzoate (870177-75-6) → ethyl 3-(3-aminopropyl)-5-(3-{4-(3-tert-butoxycarbonylaminopropoxy)-3,5-bis(1,3-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propan-2-yloxy)benzoylamino}propyl)benzoate

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; for 1h;

DOI:10.1002/chem.200401078

upstream raw materials:

4-(3-tert-butoxycarbonylaminopropoxy)-3,5-bis(1,3-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propan-2-yloxy)benzoic acid

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