ethyl,4-ethenylphenyl (1-(N-tert-butoxycarbonylamino)-2-phenyl)ethylphosphonate

Base Information

Chemical Name:ethyl,4-ethenylphenyl (1-(N-tert-butoxycarbonylamino)-2-phenyl)ethylphosphonate
CAS No.:289506-30-5
Molecular Formula:C₂₃H₃₀NO₅P
Molecular Weight:431.469
Hs Code.:

Synonyms:ethyl,4-ethenylphenyl (1-(N-tert-butoxycarbonylamino)-2-phenyl)ethylphosphonate

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Chemical Property of ethyl,4-ethenylphenyl (1-(N-tert-butoxycarbonylamino)-2-phenyl)ethylphosphonate

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Technology Process of ethyl,4-ethenylphenyl (1-(N-tert-butoxycarbonylamino)-2-phenyl)ethylphosphonate

There total 6 articles about ethyl,4-ethenylphenyl (1-(N-tert-butoxycarbonylamino)-2-phenyl)ethylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 2628-17-3,24979-70-2
4-Vinylphenol

: 289506-29-2
H,ethyl (1-(N-tert-butoxycarbonylamino)-2-phenyl)ethylphosphonate

: 289506-30-5
ethyl,4-ethenylphenyl (1-(N-tert-butoxycarbonylamino)-2-phenyl)ethylphosphonate

Guidance literature:: With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In dichloromethane;
DOI:10.1021/jo000014n

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 289506-30-5
ethyl,4-ethenylphenyl (1-(N-tert-butoxycarbonylamino)-2-phenyl)ethylphosphonate

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / tetrahydrofuran / Heating

2: 89 percent / Na / 2 h / 20 °C

3: 75 percent / aq. NaOH / ethanol / 70 °C

4: 100 percent / [benzotriazol-1-yloxy-tris(dimethylamino)phosphonium]PF₆; Et₃N / CH₂Cl₂

With sodium hydroxide; sodium; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In tetrahydrofuran; ethanol; dichloromethane; 1: Acylation / 2: Substitution / 3: Hydrolysis / 4: Condensation;
DOI:10.1021/jo000014n

Reference yield:

: 73270-44-7
diphenyl (1-amino-2-phenyl)ethylphosphonate

: 289506-30-5
ethyl,4-ethenylphenyl (1-(N-tert-butoxycarbonylamino)-2-phenyl)ethylphosphonate

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / tetrahydrofuran / Heating

2: 89 percent / Na / 2 h / 20 °C

3: 75 percent / aq. NaOH / ethanol / 70 °C

4: 100 percent / [benzotriazol-1-yloxy-tris(dimethylamino)phosphonium]PF₆; Et₃N / CH₂Cl₂

With sodium hydroxide; sodium; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In tetrahydrofuran; ethanol; dichloromethane; 1: Acylation / 2: Substitution / 3: Hydrolysis / 4: Condensation;
DOI:10.1021/jo000014n