(1S,2R,3S,4R,5R)-N-(benzyloxycarbonyl)-2,3,4-trihydroxy-6-oxa-nor-tropane

Base Information

Chemical Name:(1S,2R,3S,4R,5R)-N-(benzyloxycarbonyl)-2,3,4-trihydroxy-6-oxa-nor-tropane
CAS No.:383369-46-8
Molecular Formula:C₁₄H₁₇NO₆
Molecular Weight:295.292
Hs Code.:

Synonyms:(1S,2R,3S,4R,5R)-N-(benzyloxycarbonyl)-2,3,4-trihydroxy-6-oxa-nor-tropane

Suppliers and Price of (1S,2R,3S,4R,5R)-N-(benzyloxycarbonyl)-2,3,4-trihydroxy-6-oxa-nor-tropane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (1S,2R,3S,4R,5R)-N-(benzyloxycarbonyl)-2,3,4-trihydroxy-6-oxa-nor-tropane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (1S,2R,3S,4R,5R)-N-(benzyloxycarbonyl)-2,3,4-trihydroxy-6-oxa-nor-tropane

There total 3 articles about (1S,2R,3S,4R,5R)-N-(benzyloxycarbonyl)-2,3,4-trihydroxy-6-oxa-nor-tropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 129279-37-4
5-benzyloxycarbonylamino-5-deoxy-1,2-O-isopropylidene-β-L-ido-1,4-furanose

: 383369-46-8
(1S,2R,3S,4R,5R)-N-(benzyloxycarbonyl)-2,3,4-trihydroxy-6-oxa-nor-tropane

Guidance literature:: 5-benzyloxycarbonylamino-5-deoxy-1,2-O-isopropylidene-β-L-ido-1,4-furanose; With trifluoroacetic acid; at 20 ℃;

With Amberlite IRA 68 (OH^-); In water; Further stages.;
DOI:10.1021/jo015639f

Reference yield:

: 14685-99-5
(-)-5-amino-5-deoxy-1,2-O-isopropylidene-β-L-idofuranose

: 383369-46-8
(1S,2R,3S,4R,5R)-N-(benzyloxycarbonyl)-2,3,4-trihydroxy-6-oxa-nor-tropane

Guidance literature:: Multi-step reaction with 2 steps

1.1: 85 percent / Na₂CO₃ / H₂O / 2.17 h / 0 - 20 °C / pH 8

2.1: aq. TFA / 20 °C

2.2: 80 percent / Amberlite IRA 68 (OH^-) / H₂O

With sodium carbonate; trifluoroacetic acid; In water;
DOI:10.1021/jo015639f

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 383369-46-8
(1S,2R,3S,4R,5R)-N-(benzyloxycarbonyl)-2,3,4-trihydroxy-6-oxa-nor-tropane

Guidance literature:: Multi-step reaction with 2 steps

1.1: 85 percent / Na₂CO₃ / H₂O / 2.17 h / 0 - 20 °C / pH 8

2.1: aq. TFA / 20 °C

2.2: 80 percent / Amberlite IRA 68 (OH^-) / H₂O

With sodium carbonate; trifluoroacetic acid; In water;
DOI:10.1021/jo015639f