N¹-(2,3-Di-O-benzoyl-β-D-ribofuranosyluronsaeure-methylester)-(1->N¹)-uracil

Base Information

• Chemical Name: N¹-(2,3-Di-O-benzoyl-β-D-ribofuranosyluronsaeure-methylester)-(1->N¹)-uracil
• CAS No.: 74293-75-7
• Molecular Formula: C₂₄H₂₀N₂O₉
• Molecular Weight: 480.431

Synonyms:N¹-(2,3-Di-O-benzoyl-β-D-ribofuranosyluronsaeure-methylester)-(1->N¹)-uracil

Chemical Property of N¹-(2,3-Di-O-benzoyl-β-D-ribofuranosyluronsaeure-methylester)-(1->N¹)-uracil

Chemical Property:

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Technology Process of N¹-(2,3-Di-O-benzoyl-β-D-ribofuranosyluronsaeure-methylester)-(1->N¹)-uracil

There total 3 articles about N¹-(2,3-Di-O-benzoyl-β-D-ribofuranosyluronsaeure-methylester)-(1->N¹)-uracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

(2S,3R,4R,5S)-3,4-Bis-benzoyloxy-5-chloro-tetrahydro-furan-2-carboxylic acid methyl ester (72086-38-5) + O,O'-bis-(trimethylsilyl)uracil (10457-14-4) → N1-(2,3-Di-O-benzoyl-β-D-ribofuranosyluronsaeure-methylester)-(1->N1)-uracil (74293-75-7)

Guidance literature:

With silver perchlorate; In benzene; at 25 ℃; for 18h;

Reference yield:

(2S,3R,4R,5S)-3,4-Bis-benzoyloxy-5-chloro-tetrahydro-furan-2-carboxylic acid methyl ester (72086-38-5) + O,O'-bis-(trimethylsilyl)uracil (10457-14-4) → N3-(2,3-Di-O-benzoyl-β-D-ribofuranosyluronsaeure-methylester)-(1->N3)-uracil (74293-76-8) + N1-(2,3-Di-O-benzoyl-β-D-ribofuranosyluronsaeure-methylester)-(1->N1)-uracil (74293-75-7)

Guidance literature:

With tin(IV) chloride; In 1,2-dichloro-ethane; at 25 ℃; for 21h; Yield given. Yields of byproduct given;

Reference yield:

(2S,3R,4R,5S)-3,4-Bis-benzoyloxy-5-chloro-tetrahydro-furan-2-carboxylic acid methyl ester (72086-38-5) + O,O'-bis-(trimethylsilyl)uracil (10457-14-4) → N1-(2,3-Di-O-benzoyl-α-D-ribofuranosyluronsaeure-methylester)-(1->N1)-uracil (74293-74-6) + N1-(2,3-Di-O-benzoyl-β-D-ribofuranosyluronsaeure-methylester)-(1->N1)-uracil (74293-75-7)

Guidance literature:

at 110 ℃; for 6h; under 40 - 50 Torr; Yield given. Yields of byproduct given;

upstream raw materials:

(2S,3R,4R,5S)-3,4-Bis-benzoyloxy-5-chloro-tetrahydro-furan-2-carboxylic acid methyl ester

O,O'-bis-(trimethylsilyl)uracil

Downstream raw materials:

N¹-(β-D-Ribofuranosyluronsaeure-methylester)-(1->N¹)-uracil

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