Technology Process of C47H61N5O10
There total 10 articles about C47H61N5O10 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dmap; 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
acetonitrile;
at 20 ℃;
for 16h;
DOI:10.1016/j.bmcl.2011.01.084
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 2,4,6-trichlorobenzoyl chloride; N-ethyl-N,N-diisopropylamine / tetrahydrofuran; toluene / 1 h
1.2: 16.5 h / 20 - 110 °C
2.1: hydrogen bromide; acetic acid / dichloromethane / 0.5 h / 20 °C
3.1: dmap; 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / acetonitrile / 16 h / 20 °C
With
dmap; 1-hydroxy-7-aza-benzotriazole; 2,4,6-trichlorobenzoyl chloride; hydrogen bromide; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane; toluene; acetonitrile;
1.1: Yamaguchi reaction / 1.2: Yamaguchi reaction;
DOI:10.1016/j.bmcl.2011.01.084
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogen bromide; acetic acid / dichloromethane / 0.5 h / 20 °C
2: dmap; 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / acetonitrile / 16 h / 20 °C
With
dmap; 1-hydroxy-7-aza-benzotriazole; hydrogen bromide; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2011.01.084
