O-(3,4-Dichlorophenyl)carbamoyl-2-methylaminocyclohexanone oxime

Base Information

Chemical Name:O-(3,4-Dichlorophenyl)carbamoyl-2-methylaminocyclohexanone oxime
CAS No.:90713-81-8
Molecular Formula:C₂₁H₂₀Cl₄N₄O₃
Molecular Weight:518.227
Hs Code.:

O-(3,4-Dichlorophenyl)carbamoyl-2-<N-(3,4-dichlorophenyl)carbamoyl>methylaminocyclohexanone oxime

Synonyms:O-(3,4-Dichlorophenyl)carbamoyl-2-methylaminocyclohexanone oxime

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Chemical Property of O-(3,4-Dichlorophenyl)carbamoyl-2-methylaminocyclohexanone oxime

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Technology Process of O-(3,4-Dichlorophenyl)carbamoyl-2-methylaminocyclohexanone oxime

There total 1 articles about O-(3,4-Dichlorophenyl)carbamoyl-2-methylaminocyclohexanone oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 90713-77-2
2-Methylaminocyclohexanone E-oxime

: 102-36-3
3,4-dichlorophenylisocyanate

: 90713-81-8
O-(3,4-Dichlorophenyl)carbamoyl-2-methylaminocyclohexanone oxime

Guidance literature:: In tetrahydrofuran; for 2.33333h; Ambient temperature;
DOI:10.1007/BF00515649

Reference yield: 70.0%

: 90713-81-8
O-(3,4-Dichlorophenyl)carbamoyl-2-methylaminocyclohexanone oxime

: 90713-85-2
O-(3,4-Dichlorophenyl)carbamoyl-N-<1-methyl-3-(3,4-dichlorophenyl)-4,5-tetramethyleneimidazolidin-2-on-4-yl>hydroxylamine

Guidance literature:: With sodium hydroxide; at 70 ℃; for 0.333333h;
DOI:10.1007/BF00515649

Reference yield:

: 90713-81-8
O-(3,4-Dichlorophenyl)carbamoyl-2-methylaminocyclohexanone oxime

: 90713-89-6
4,5-Tetramethylene-1-methyl-3-(3,4-dichlorophenyl)-Δ⁴-imidazolin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / aq. NaOH, 5percent / 0.33 h / 70 °C

2: triethylamine, ethyl chlorocarbonate / CHCl₃ / 1) 25 deg C, 20 min; 2) 20 deg C, 3 h;

With sodium hydroxide; chloroformic acid ethyl ester; triethylamine; In chloroform;
DOI:10.1007/BF00515649