C₁₆H₂₄⁽²⁾HBO₂

Base Information

Chemical Name:C₁₆H₂₄⁽²⁾HBO₂
CAS No.:1438827-46-3
Molecular Formula:C₁₆H₂₅BO₂
Molecular Weight:261.176
Hs Code.:

C<sub>16</sub>H<sub>24</sub><sup>(2)</sup>HBO<sub>2</sub>

Synonyms:C₁₆H₂₄⁽²⁾HBO₂

Suppliers and Price of C₁₆H₂₄⁽²⁾HBO₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₆H₂₄⁽²⁾HBO₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₆H₂₄⁽²⁾HBO₂

There total 5 articles about C₁₆H₂₄⁽²⁾HBO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1438826-22-2
C₁₈H₃₁BO₂Si

: 1438827-46-3
C₁₆H₂₄⁽²⁾HBO₂

Guidance literature:: With chloro-trimethyl-silane; water-d2; potassium iodide; In acetonitrile; at 25 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ja403462b

Reference yield:

: 71813-50-8
1-bromo-2-(but-3-enyl)benzene

: 1438827-46-3
C₁₆H₂₄⁽²⁾HBO₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: 2-Nitrobenzenesulfonyl chloride; hydrazine hydrate / acetonitrile / 18 h / 0 - 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

2.2: 24 h / -78 - 20 °C / Inert atmosphere; Glovebox

3.1: (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 3,4,7,8-Tetramethyl-o-phenanthrolin / tetrahydrofuran / 18 h / 80 °C / Inert atmosphere; Glovebox

4.1: chloro-trimethyl-silane; potassium iodide; water-d2 / acetonitrile / 2 h / 25 °C / Inert atmosphere

With n-butyllithium; chloro-trimethyl-silane; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 3,4,7,8-Tetramethyl-o-phenanthrolin; water-d2; hydrazine hydrate; 2-Nitrobenzenesulfonyl chloride; potassium iodide; In tetrahydrofuran; hexane; acetonitrile;
DOI:10.1021/ja403462b

Reference yield:

: 13397-98-3
1-bromo-2-butylbenzene

: 1438827-46-3
C₁₆H₂₄⁽²⁾HBO₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

1.2: 24 h / -78 - 20 °C / Inert atmosphere; Glovebox

2.1: (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 3,4,7,8-Tetramethyl-o-phenanthrolin / tetrahydrofuran / 18 h / 80 °C / Inert atmosphere; Glovebox

3.1: chloro-trimethyl-silane; potassium iodide; water-d2 / acetonitrile / 2 h / 25 °C / Inert atmosphere

With n-butyllithium; chloro-trimethyl-silane; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 3,4,7,8-Tetramethyl-o-phenanthrolin; water-d2; potassium iodide; In tetrahydrofuran; hexane; acetonitrile;
DOI:10.1021/ja403462b