(2S,3S,6S)-3,6-Dihydroxy-2,6,10-trimethyl-12-(2,2,6-trimethyl-cyclohexyl)-dodecanoic acid methyl ester

Base Information

Chemical Name:(2S,3S,6S)-3,6-Dihydroxy-2,6,10-trimethyl-12-(2,2,6-trimethyl-cyclohexyl)-dodecanoic acid methyl ester
CAS No.:102843-66-3
Molecular Formula:C₂₅H₄₈O₄
Molecular Weight:412.654
Hs Code.:

Synonyms:(2S,3S,6S)-3,6-Dihydroxy-2,6,10-trimethyl-12-(2,2,6-trimethyl-cyclohexyl)-dodecanoic acid methyl ester

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Chemical Property of (2S,3S,6S)-3,6-Dihydroxy-2,6,10-trimethyl-12-(2,2,6-trimethyl-cyclohexyl)-dodecanoic acid methyl ester

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Technology Process of (2S,3S,6S)-3,6-Dihydroxy-2,6,10-trimethyl-12-(2,2,6-trimethyl-cyclohexyl)-dodecanoic acid methyl ester

There total 2 articles about (2S,3S,6S)-3,6-Dihydroxy-2,6,10-trimethyl-12-(2,2,6-trimethyl-cyclohexyl)-dodecanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 102917-97-5
(-)-epimuqubilin A methyl ester

: 102843-66-3
(2S,3S,6S)-3,6-Dihydroxy-2,6,10-trimethyl-12-(2,2,6-trimethyl-cyclohexyl)-dodecanoic acid methyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In diethyl ether; for 4h; under 760 Torr;
DOI:10.1016/S0040-4020(01)96691-8

Reference yield:

: 102917-90-8
(S)-2-{(3S,6S)-6-Methyl-6-[(E)-4-methyl-6-(2,6,6-trimethyl-cyclohex-1-enyl)-hex-3-enyl]-[1,2]dioxan-3-yl}-propionic acid

: 102843-66-3
(2S,3S,6S)-3,6-Dihydroxy-2,6,10-trimethyl-12-(2,2,6-trimethyl-cyclohexyl)-dodecanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

2: 61 percent / H₂ / 10percent Pd/C / diethyl ether / 4 h / 760 Torr

With hydrogen; palladium on activated charcoal; In diethyl ether;
DOI:10.1016/S0040-4020(01)96691-8

Reference yield: 100.0%

: 1519-21-7
2-phenylbutyric anhydride

: 102843-66-3
(2S,3S,6S)-3,6-Dihydroxy-2,6,10-trimethyl-12-(2,2,6-trimethyl-cyclohexyl)-dodecanoic acid methyl ester

: 90-27-7
2-Phenylbutyric acid

: (2S,3S,6S)-6-Hydroxy-2,6,10-trimethyl-3-(2-phenyl-butyryloxy)-12-(2,2,6-trimethyl-cyclohexyl)-dodecanoic acid methyl ester

Guidance literature:: With pyridine; for 48h; Ambient temperature; determination of the absolute configuration (according to Horeau); implied stereochemistry at C₃ is S;
DOI:10.1016/S0040-4020(01)96691-8