C₂₉H₅₂O₇SSi

Base Information

Chemical Name:C₂₉H₅₂O₇SSi
CAS No.:1610030-12-0
Molecular Formula:C₂₉H₅₂O₇SSi
Molecular Weight:572.879
Hs Code.:

C<sub>29</sub>H<sub>52</sub>O<sub>7</sub>SSi

Synonyms:C₂₉H₅₂O₇SSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₅₂O₇SSi

Chemical Property:

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Technology Process of C₂₉H₅₂O₇SSi

There total 8 articles about C₂₉H₅₂O₇SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106-88-7
ethyloxirane

: 1610029-90-7
C₂₅H₄₄O₆SSi

: 1610030-12-0
C₂₉H₅₂O₇SSi

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; at 0 - 20 ℃; for 6h; Inert atmosphere;
DOI:10.1021/ol5006856

Reference yield:

: {(2R,3R)-3-[(R)-2-(4-Methoxy-benzyloxy)-1-methyl-ethyl]-oxiranyl}-methanol

: 1610030-12-0
C₂₉H₅₂O₇SSi

Guidance literature:: Multi-step reaction with 12 steps

1.1: sodium bis(2-methoxyethoxy)aluminium dihydride / dichloromethane; toluene / 22 h / 0 - 20 °C / Inert atmosphere

1.2: 1 h / 20 °C

2.1: pyridine / dichloromethane / 17 h / 0 - 20 °C / Inert atmosphere

3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 2 h / 20 °C

4.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 2 h / 20 °C / Inert atmosphere

5.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / tetrahydrofuran / 168 h / 20 °C

6.1: diisobutylaluminium hydride / tetrahydrofuran; hexane / 1.5 h / -72 °C / Inert atmosphere

7.1: titanium(IV) isopropylate; diethyl (2R,3R)-tartrate / dichloromethane / 0.75 h / -30 °C / Molecular sieve; Inert atmosphere

7.2: 15 h / -30 °C / Molecular sieve; Inert atmosphere

8.1: pyridine; tributylphosphine / 6.5 h / 20 - 50 °C / Inert atmosphere

9.1: dichloromethane; hexane / 19 h / -50 °C / Inert atmosphere

10.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 50 h / 20 °C / Inert atmosphere

11.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.75 h / 0 °C

12.1: lithium hexamethyldisilazane / tetrahydrofuran / 6 h / 0 - 20 °C / Inert atmosphere

With pyridine; titanium(IV) isopropylate; diethyl (2R,3R)-tartrate; tributylphosphine; diisobutylaluminium hydride; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; sodium bis(2-methoxyethoxy)aluminium dihydride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium hexamethyldisilazane; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; hexane; dichloromethane; water; dimethyl sulfoxide; toluene; 5.1: |Wittig Olefination / 7.1: |Sharpless Asymmetric Epoxidation / 7.2: |Sharpless Asymmetric Epoxidation;
DOI:10.1021/ol5006856

Reference yield:

: C₁₄H₂₈O₃Si

: 1610030-12-0
C₂₉H₅₂O₇SSi

Guidance literature:: Multi-step reaction with 8 steps

1.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / tetrahydrofuran / 168 h / 20 °C

2.1: diisobutylaluminium hydride / tetrahydrofuran; hexane / 1.5 h / -72 °C / Inert atmosphere

3.1: titanium(IV) isopropylate; diethyl (2R,3R)-tartrate / dichloromethane / 0.75 h / -30 °C / Molecular sieve; Inert atmosphere

3.2: 15 h / -30 °C / Molecular sieve; Inert atmosphere

4.1: pyridine; tributylphosphine / 6.5 h / 20 - 50 °C / Inert atmosphere

5.1: dichloromethane; hexane / 19 h / -50 °C / Inert atmosphere

6.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 50 h / 20 °C / Inert atmosphere

7.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.75 h / 0 °C

8.1: lithium hexamethyldisilazane / tetrahydrofuran / 6 h / 0 - 20 °C / Inert atmosphere

With pyridine; titanium(IV) isopropylate; diethyl (2R,3R)-tartrate; tributylphosphine; diisobutylaluminium hydride; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium hexamethyldisilazane; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; hexane; dichloromethane; 1.1: |Wittig Olefination / 3.1: |Sharpless Asymmetric Epoxidation / 3.2: |Sharpless Asymmetric Epoxidation;
DOI:10.1021/ol5006856