BETA1,BETA3-DIOXO-1,3-BENZENEDIPROPANOIC ACID 1,3-DIMETHYL ESTER

Base Information

Chemical Name:BETA1,BETA3-DIOXO-1,3-BENZENEDIPROPANOIC ACID 1,3-DIMETHYL ESTER
CAS No.:75160-05-3
Molecular Formula:C₁₄H₁₄O₆
Molecular Weight:278.262
Hs Code.:
Mol file:75160-05-3.mol

Synonyms:3,3'-dioxo-3,3'-m-phenylene-di-propionic acid dimethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of BETA1,BETA3-DIOXO-1,3-BENZENEDIPROPANOIC ACID 1,3-DIMETHYL ESTER

Chemical Property:

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Technology Process of BETA1,BETA3-DIOXO-1,3-BENZENEDIPROPANOIC ACID 1,3-DIMETHYL ESTER

There total 6 articles about BETA1,BETA3-DIOXO-1,3-BENZENEDIPROPANOIC ACID 1,3-DIMETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 38330-80-2
monomethyl monopotassium malonate

: 23449-84-5
isophthaloyl diimidazole

: C₁₄H₁₄O₆

: C₁₄H₁₄O₆

: 75160-05-3
3,3'-dioxo-3,3'-m-phenylene-di-propionic acid dimethyl ester

Guidance literature:: monomethyl monopotassium malonate; With magnesium chloride; In tetrahydrofuran; at 65 ℃; for 5h; Inert atmosphere;

isophthaloyl diimidazole; In tetrahydrofuran; at 30 ℃; for 24h; Inert atmosphere;
DOI:10.1039/b913336d

Reference yield:

: 159279-96-6
m-phenylenedi-propiolic acid dimethyl ester

: 75160-05-3
3,3'-dioxo-3,3'-m-phenylene-di-propionic acid dimethyl ester

Guidance literature:: With sulfuric acid; Eintragen des Reaktionsgemisches in Wasser;
DOI:10.1002/hlca.193601901127

Reference yield:

: 23746-59-0
(E)-3-[3-((E)-2-methoxycarbonyl-vinyl)-phenyl]-acrylic acid methyl ester

: 75160-05-3
3,3'-dioxo-3,3'-m-phenylene-di-propionic acid dimethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: ethyl acetate; bromine

2: ethanolic KOH-solution

3: sulfuric acid

4: sulfuric acid / Eintragen des Reaktionsgemisches in Wasser

With potassium hydroxide; sulfuric acid; bromine; ethyl acetate;
DOI:10.1002/hlca.193601901127