N-<(2R)-2-(1-Naphthylmethyl)-3-(N-phenethylcarbamoyl)propionyl>-L-histidine Hydrazide

Base Information

Chemical Name:N-<(2R)-2-(1-Naphthylmethyl)-3-(N-phenethylcarbamoyl)propionyl>-L-histidine Hydrazide
CAS No.:105227-75-6
Molecular Formula:C₂₉H₃₂N₆O₃
Molecular Weight:512.611
Hs Code.:

Synonyms:N-<(2R)-2-(1-Naphthylmethyl)-3-(N-phenethylcarbamoyl)propionyl>-L-histidine Hydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<(2R)-2-(1-Naphthylmethyl)-3-(N-phenethylcarbamoyl)propionyl>-L-histidine Hydrazide

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Technology Process of N-<(2R)-2-(1-Naphthylmethyl)-3-(N-phenethylcarbamoyl)propionyl>-L-histidine Hydrazide

There total 3 articles about N-<(2R)-2-(1-Naphthylmethyl)-3-(N-phenethylcarbamoyl)propionyl>-L-histidine Hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 132488-68-7
N-<(2R)-2-(1-naphthylmethyl)-3-(N-phenethylcarbamoyl)propionyl>-L-histidine methyl ester

: 105227-75-6
N-<(2R)-2-(1-Naphthylmethyl)-3-(N-phenethylcarbamoyl)propionyl>-L-histidine Hydrazide

Guidance literature:: With hydrazine hydrate; In methanol; overnight;
DOI:10.1248/cpb.38.3042

Reference yield:

: 120052-26-8
(R)-2-(1-Naphthylmethyl)-3-(N-phenethylcarbamoyl)propionic Acid

: 105227-75-6
N-<(2R)-2-(1-Naphthylmethyl)-3-(N-phenethylcarbamoyl)propionyl>-L-histidine Hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / Et₃N, diphenylphosphoryl azide / dimethylformamide / 16 h / 0 °C

2: 93 percent / hydrazine hydrate / methanol / overnight

With diphenylphosphoranyl azide; hydrazine hydrate; triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1248/cpb.38.3042

Reference yield:

: 4467-54-3,5619-10-3,7389-87-9,18684-16-7,22888-60-4,32381-17-2,92742-29-5,100009-20-9
l-histidine methyl ester dihydrochloride

: 105227-75-6
N-<(2R)-2-(1-Naphthylmethyl)-3-(N-phenethylcarbamoyl)propionyl>-L-histidine Hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / Et₃N, diphenylphosphoryl azide / dimethylformamide / 16 h / 0 °C

2: 93 percent / hydrazine hydrate / methanol / overnight

With diphenylphosphoranyl azide; hydrazine hydrate; triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1248/cpb.38.3042