Cl₂BCHCCl(C₆H₄F)

Base Information

• Chemical Name: Cl₂BCHCCl(C₆H₄F)
• CAS No.: 1018853-10-5
• Molecular Formula: C₈H₅BCl₃F
• Molecular Weight: 237.296

Synonyms:Cl₂BCHCCl(C₆H₄F)

Chemical Property of Cl₂BCHCCl(C₆H₄F)

Chemical Property:

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Technology Process of Cl₂BCHCCl(C₆H₄F)

There total 1 articles about Cl₂BCHCCl(C₆H₄F) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-ethynyl-3-fluoro-benzene (2561-17-3) → Cl2BCHCCl(C6H4F) (1018853-10-5)

Guidance literature:

With boron trichloride; In dichloromethane; for 1h;

DOI:10.1039/b502026c

Reference yield: 78.0%

Cl2BCHCCl(C6H4F) (1018853-10-5) + (E)-1,3-diphenyl-2-propen-1-ol (62668-02-4) → 1-((1Z,4E)-1-Chloro-3,5-diphenyl-penta-1,4-dienyl)-3-fluoro-benzene

Guidance literature:

With n-butyllithium; In hexane; dichloromethane; at 20 ℃;

DOI:10.1055/s-2007-990816

Reference yield:

Cl2BCHCCl(C6H4F) (1018853-10-5) + ethyl (E)-1-phenylbut-1-en-3-ol (36004-04-3) → 1-((1Z,4E)-1-Chloro-3-methyl-5-phenyl-penta-1,4-dienyl)-3-fluoro-benzene

Guidance literature:

ethyl (E)-1-phenylbut-1-en-3-ol; With n-butyllithium; In hexane; dichloromethane; at 20 ℃; for 1h;

Cl₂BCHCCl(C₆H₄F); In hexane; dichloromethane; at 20 ℃;

DOI:10.1039/b502026c

upstream raw materials:

1-ethynyl-3-fluoro-benzene

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