(4-tert-butyl-2,6-bis[(2,2'',6,6''-tetramethyl-m-terphenyl-2'-yl)-methyl]phenyl)Br

Base Information

Chemical Name:(4-tert-butyl-2,6-bis[(2,2'',6,6''-tetramethyl-m-terphenyl-2'-yl)-methyl]phenyl)Br
CAS No.:177971-43-6
Molecular Formula:C₅₆H₅₇Br
Molecular Weight:809.973
Hs Code.:

Synonyms:(4-tert-butyl-2,6-bis[(2,2'',6,6''-tetramethyl-m-terphenyl-2'-yl)-methyl]phenyl)Br

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Chemical Property of (4-tert-butyl-2,6-bis[(2,2'',6,6''-tetramethyl-m-terphenyl-2'-yl)-methyl]phenyl)Br

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Technology Process of (4-tert-butyl-2,6-bis[(2,2'',6,6''-tetramethyl-m-terphenyl-2'-yl)-methyl]phenyl)Br

There total 1 articles about (4-tert-butyl-2,6-bis[(2,2'',6,6''-tetramethyl-m-terphenyl-2'-yl)-methyl]phenyl)Br which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 96929-82-7
2-bromo-1,3-bis(bromomethyl)-5-tert-butylbenzene

: 129678-40-6
2'-iodo-2,6,2,6-tetramethyl-1,1':3',1-terphenyl

: 177971-43-6
(4-tert-butyl-2,6-bis[(2,2'',6,6''-tetramethyl-m-terphenyl-2'-yl)-methyl]phenyl)Br

Guidance literature:: 2'-iodo-2,6,2",6"-tetramethyl-1,1':3',1"-terphenyl; With magnesium; In tetrahydrofuran; at 14 ℃;

2-bromo-1,3-bis(bromomethyl)-5-tert-butylbenzene; With lithium chloride; copper dichloride; In tetrahydrofuran; for 14h; Further stages.; Heating;
DOI:10.1039/b006647h

Reference yield: 80.0%

: 16842-00-5,855944-65-9
trimethylamine alane

: 177971-43-6
(4-tert-butyl-2,6-bis[(2,2'',6,6''-tetramethyl-m-terphenyl-2'-yl)-methyl]phenyl)Br

: Li(CH₃OCH₂CH₂OCH₃)2⁽¹⁺⁾*C₅₆H₅₇AlH₃^(1-)=C₅₆H₅₇AlH₃Li(CH₃OCH₂CH₂OCH₃)2

Guidance literature:: With t-BuLi; In 1,2-dimethoxyethane; pentane; benzene; t-BuLi soln. (pentane) dropwise addn. to ligand soln. (DME, -72°C), stirring (8 min), Al-compd. soln. (C6H6) addn., stirring (-72°C, overnight), evapn. (room temp.); recrystn. (DME, Ar-atmosphere); elem. anal.;

Reference yield: 74.0%

: 75-15-0,12122-00-8
carbon disulfide

: 177971-43-6
(4-tert-butyl-2,6-bis[(2,2'',6,6''-tetramethyl-m-terphenyl-2'-yl)-methyl]phenyl)Br

: 877465-02-6
dithioformic acid 4-tert-butyl-2,6-bis-(2,6,2'',6''-tetramethyl-[1,1';3',1'']terphenyl-2'-ylmethyl)-phenyl ester

Guidance literature:: (4-tert-butyl-2,6-bis[(2,2'',6,6''-tetramethyl-m-terphenyl-2'-yl)-methyl]phenyl)Br; With tert.-butyl lithium; at -78 ℃;

carbon disulfide; at -78 ℃;
DOI:10.1246/cl.2005.1674