2-[2-[(1-benzyl-1H-1,2,3-triazol-4-yl)methoxy]phenyl]-5-methylbenzoxazole

Base Information

Chemical Name:2-[2-[(1-benzyl-1H-1,2,3-triazol-4-yl)methoxy]phenyl]-5-methylbenzoxazole
CAS No.:1451257-04-7
Molecular Formula:C₂₄H₂₀N₄O₂
Molecular Weight:396.448
Hs Code.:

Synonyms:2-[2-[(1-benzyl-1H-1,2,3-triazol-4-yl)methoxy]phenyl]-5-methylbenzoxazole

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Chemical Property of 2-[2-[(1-benzyl-1H-1,2,3-triazol-4-yl)methoxy]phenyl]-5-methylbenzoxazole

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Technology Process of 2-[2-[(1-benzyl-1H-1,2,3-triazol-4-yl)methoxy]phenyl]-5-methylbenzoxazole

There total 4 articles about 2-[2-[(1-benzyl-1H-1,2,3-triazol-4-yl)methoxy]phenyl]-5-methylbenzoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1451257-09-2
5-methyl-2-[2-(prop-2-yn-1-yloxy)phenyl]-1,3-benzoxazole

: 622-79-7
benzyl azide

: 1451257-04-7
2-[2-[(1-benzyl-1H-1,2,3-triazol-4-yl)methoxy]phenyl]-5-methylbenzoxazole

Guidance literature:: With 5% Cu2O/C; triethylamine; In water; isopropyl alcohol; for 4h; Reflux;
DOI:10.3998/ark.5550190.0014.312

Reference yield:

: 35875-76-4
5-methyl-2-(2-hydroxyphenyl)benzoxazole

: 1451257-04-7
2-[2-[(1-benzyl-1H-1,2,3-triazol-4-yl)methoxy]phenyl]-5-methylbenzoxazole

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone

2: 5% Cu2O/C; triethylamine / water; isopropyl alcohol / 4 h / Reflux

With 5% Cu2O/C; potassium carbonate; triethylamine; In water; isopropyl alcohol; acetone; 2: |Huisgen Cycloaddition;
DOI:10.3998/ark.5550190.0014.312

Reference yield:

: 90-02-8
salicylaldehyde

: 1451257-04-7
2-[2-[(1-benzyl-1H-1,2,3-triazol-4-yl)methoxy]phenyl]-5-methylbenzoxazole

Guidance literature:: Multi-step reaction with 3 steps

1: potassium cyanide; phenylboronic acid / methanol / 20 °C

2: potassium carbonate / acetone

3: 5% Cu2O/C; triethylamine / water; isopropyl alcohol / 4 h / Reflux

With potassium cyanide; 5% Cu2O/C; potassium carbonate; triethylamine; phenylboronic acid; In methanol; water; isopropyl alcohol; acetone; 3: |Huisgen Cycloaddition;
DOI:10.3998/ark.5550190.0014.312