(S)-7-bromo-3-phenyl-3,4-dihydro-2H-benzo[b][1,4,5]oxathiazepine 1,1-dioxide

Base Information

Chemical Name:(S)-7-bromo-3-phenyl-3,4-dihydro-2H-benzo[b][1,4,5]oxathiazepine 1,1-dioxide
CAS No.:1233355-08-2
Molecular Formula:C₁₄H₁₂BrNO₃S
Molecular Weight:354.224
Hs Code.:

Synonyms:(S)-7-bromo-3-phenyl-3,4-dihydro-2H-benzo[b][1,4,5]oxathiazepine 1,1-dioxide

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Chemical Property of (S)-7-bromo-3-phenyl-3,4-dihydro-2H-benzo[b][1,4,5]oxathiazepine 1,1-dioxide

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Technology Process of (S)-7-bromo-3-phenyl-3,4-dihydro-2H-benzo[b][1,4,5]oxathiazepine 1,1-dioxide

There total 1 articles about (S)-7-bromo-3-phenyl-3,4-dihydro-2H-benzo[b][1,4,5]oxathiazepine 1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1257313-53-3
C₁₄H₁₃BrFNO₃S

: 1233355-08-2
(S)-7-bromo-3-phenyl-3,4-dihydro-2H-benzo[b][1,4,5]oxathiazepine 1,1-dioxide

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 140 ℃; Microwave irradiation;
DOI:10.1002/chem.201001651

Reference yield:

: 1233355-08-2
(S)-7-bromo-3-phenyl-3,4-dihydro-2H-benzo[b][1,4,5]oxathiazepine 1,1-dioxide

: 1233656-18-2
C₁₆H₁₉O₄P

: 1233355-12-8
(S)-2-benzyl-7-bromo-3-phenyl-3,4-dihydro-2H-benzo[b][1,4,5]oxathiazepine 1,1-dioxide

Guidance literature:: C₁₆H₁₉O₄P; With Grubbs catalyst first generation; In dichloromethane; at 50 ℃; Inert atmosphere;

(S)-7-bromo-3-phenyl-3,4-dihydro-2H-benzo[b][1,4,5]oxathiazepine 1,1-dioxide; With tetra-(n-butyl)ammonium iodide; potassium carbonate; In tetrahydrofuran; at 80 ℃; Inert atmosphere;
DOI:10.1021/ol1006604

Reference yield:

: 1233355-08-2
(S)-7-bromo-3-phenyl-3,4-dihydro-2H-benzo[b][1,4,5]oxathiazepine 1,1-dioxide

: 1233656-26-2
C₁₈H₂₃O₆P

: 1233355-13-9
(S)-7-bromo-2-(3,5-dimethoxybenzyl)-3-phenyl-3,4-dihydro-2H-benzo[b][1,4,5]oxathiazepine 1,1-dioxide

Guidance literature:: C₁₈H₂₃O₆P; With Grubbs catalyst first generation; In dichloromethane; at 50 ℃; Inert atmosphere;

(S)-7-bromo-3-phenyl-3,4-dihydro-2H-benzo[b][1,4,5]oxathiazepine 1,1-dioxide; With tetra-(n-butyl)ammonium iodide; potassium carbonate; In tetrahydrofuran; at 80 ℃; Inert atmosphere;
DOI:10.1021/ol1006604