O-{1-methyl-3-[methyl(p-toluenesulfonyl)amino]butyl} O-(p-tolyl)thiocarbonate

Base Information

Chemical Name:O-{1-methyl-3-[methyl(p-toluenesulfonyl)amino]butyl} O-(p-tolyl)thiocarbonate
CAS No.:497069-42-8
Molecular Formula:C₂₁H₂₇NO₄S₂
Molecular Weight:421.582
Hs Code.:

Synonyms:O-{1-methyl-3-[methyl(p-toluenesulfonyl)amino]butyl} O-(p-tolyl)thiocarbonate

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Chemical Property of O-{1-methyl-3-[methyl(p-toluenesulfonyl)amino]butyl} O-(p-tolyl)thiocarbonate

Chemical Property:

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Technology Process of O-{1-methyl-3-[methyl(p-toluenesulfonyl)amino]butyl} O-(p-tolyl)thiocarbonate

There total 4 articles about O-{1-methyl-3-[methyl(p-toluenesulfonyl)amino]butyl} O-(p-tolyl)thiocarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 937-63-3
p-Tolyl chlorothionoformate

: 497069-44-0
N-(3-hydroxy-1-methylbutyl)-N-methyl-p-toluenesulfonamide

: 497069-42-8
O-{1-methyl-3-[methyl(p-toluenesulfonyl)amino]butyl} O-(p-tolyl)thiocarbonate

Guidance literature:: In dichloromethane; for 3h; Heating;
DOI:10.1002/1099-0690(200208)2002:16<2742::AID-EJOC2742>3.0.CO;2-R

Reference yield:

: N-(3-hydroxy-1-methylbutyl)-p-toluenesulfonamide

: 497069-42-8
O-{1-methyl-3-[methyl(p-toluenesulfonyl)amino]butyl} O-(p-tolyl)thiocarbonate

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / K₂CO₃ / acetone / 8 h / Heating

2: 97 percent / CH₂Cl₂ / 3 h / Heating

With potassium carbonate; In dichloromethane; acetone;
DOI:10.1002/1099-0690(200208)2002:16<2742::AID-EJOC2742>3.0.CO;2-R

Reference yield:

: 13325-12-7
4-amino-2-pentanol

: 497069-42-8
O-{1-methyl-3-[methyl(p-toluenesulfonyl)amino]butyl} O-(p-tolyl)thiocarbonate

Guidance literature:: Multi-step reaction with 3 steps

1: 41 percent / NEt₃ / CH₂Cl₂ / 0.75 h / 0 - 20 °C

2: 95 percent / K₂CO₃ / acetone / 8 h / Heating

3: 97 percent / CH₂Cl₂ / 3 h / Heating

With potassium carbonate; triethylamine; In dichloromethane; acetone;
DOI:10.1002/1099-0690(200208)2002:16<2742::AID-EJOC2742>3.0.CO;2-R