C₃₀H₃₇Cl₃N₄O₅S₂Si

Base Information

Chemical Name:C₃₀H₃₇Cl₃N₄O₅S₂Si
CAS No.:1061574-19-3
Molecular Formula:C₃₀H₃₇Cl₃N₄O₅S₂Si
Molecular Weight:732.224
Hs Code.:

C<sub>30</sub>H<sub>37</sub>Cl<sub>3</sub>N<sub>4</sub>O<sub>5</sub>S<sub>2</sub>Si

Synonyms:C₃₀H₃₇Cl₃N₄O₅S₂Si

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Chemical Property of C₃₀H₃₇Cl₃N₄O₅S₂Si

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Technology Process of C₃₀H₃₇Cl₃N₄O₅S₂Si

There total 6 articles about C₃₀H₃₇Cl₃N₄O₅S₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 425-75-2
trifluoromethanesulfonic acid ethyl ester

: 1061574-16-0
C₂₈H₃₃Cl₃N₄O₅S₂Si

: 1061574-19-3
C₃₀H₃₇Cl₃N₄O₅S₂Si

: C₃₀H₃₇Cl₃N₄O₅S₂Si

Guidance literature:: With 2,4,6-tri-tert-butylpyrimidine; In dichloromethane; at 37 ℃; for 29h; Reagent/catalyst; Inert atmosphere; Sealed tube;
DOI:10.1021/jacs.6b02343

Reference yield: 77.0%

: 425-75-2
trifluoromethanesulfonic acid ethyl ester

: 1061574-16-0
C₂₈H₃₃Cl₃N₄O₅S₂Si

: 1061574-19-3
C₃₀H₃₇Cl₃N₄O₅S₂Si

Guidance literature:: With 2,4,6-tri-tert-butylpyrimidine; In dichloromethane; at 37 ℃; for 14h; vessel sealed with glass stopper;

Reference yield:

: 1061574-11-5
C₉H₁₂N₂O₄

: 1061574-19-3
C₃₀H₃₇Cl₃N₄O₅S₂Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 14 h / 0 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / dichloromethane; toluene / 2 h / -90 °C / Inert atmosphere

3.1: dichloromethane / 0.33 h / 0 - 20 °C / Inert atmosphere

3.2: 1.67 h / -78 - 20 °C / Inert atmosphere

4.1: 1,3-dimethylbarbituric acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 8 h / Inert atmosphere

4.2: 0.33 h / Inert atmosphere

5.1: 2,4,6-tri-tert-butylpyrimidine / dichloromethane / 29 h / 37 °C / Inert atmosphere; Sealed tube

With 1H-imidazole; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1,3-dimethylbarbituric acid; diisobutylaluminium hydride; 2,4,6-tri-tert-butylpyrimidine; In dichloromethane; N,N-dimethyl-formamide; toluene; 3.1: |Pictet-Spengler Synthesis / 3.2: |Pictet-Spengler Synthesis;
DOI:10.1021/jacs.6b02343