5 (S), 7 (S)-BIS-(TERT-BUTYL-DIMETHYL-SILANYLOXY)-1 0 (S)-[2-(4-METH OXY-BENZYL)-5 (S)-methyl-[1, 3 [(R)]] [DIOXAN-4-YL]-4] (R)-methyl-undeca-2, [8-DIEN-1-OL]

Base Information

• Chemical Name: 5 (S), 7 (S)-BIS-(TERT-BUTYL-DIMETHYL-SILANYLOXY)-1 0 (S)-[2-(4-METH OXY-BENZYL)-5 (S)-methyl-[1, 3 [(R)]] [DIOXAN-4-YL]-4] (R)-methyl-undeca-2, [8-DIEN-1-OL]
• CAS No.: 672296-36-5
• Molecular Formula: C₃₆H₆₄O₆Si₂
• Molecular Weight: 649.072

Synonyms:5 (S), 7 (S)-BIS-(TERT-BUTYL-DIMETHYL-SILANYLOXY)-1 0 (S)-[2-(4-METH OXY-BENZYL)-5 (S)-methyl-[1, 3 [(R)]] [DIOXAN-4-YL]-4] (R)-methyl-undeca-2, [8-DIEN-1-OL]

Chemical Property of 5 (S), 7 (S)-BIS-(TERT-BUTYL-DIMETHYL-SILANYLOXY)-1 0 (S)-[2-(4-METH OXY-BENZYL)-5 (S)-methyl-[1, 3 [(R)]] [DIOXAN-4-YL]-4] (R)-methyl-undeca-2, [8-DIEN-1-OL]

Chemical Property:

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Technology Process of 5 (S), 7 (S)-BIS-(TERT-BUTYL-DIMETHYL-SILANYLOXY)-1 0 (S)-[2-(4-METH OXY-BENZYL)-5 (S)-methyl-[1, 3 [(R)]] [DIOXAN-4-YL]-4] (R)-methyl-undeca-2, [8-DIEN-1-OL]

There total 1 articles about 5 (S), 7 (S)-BIS-(TERT-BUTYL-DIMETHYL-SILANYLOXY)-1 0 (S)-[2-(4-METH OXY-BENZYL)-5 (S)-methyl-[1, 3 [(R)]] [DIOXAN-4-YL]-4] (R)-methyl-undeca-2, [8-DIEN-1-OL] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

C39H66O9Si2 → 5 (S), 7 (S)-BIS-(TERT-BUTYL-DIMETHYL-SILANYLOXY)-1 0 (S)-[2-(4-METH OXY-BENZYL)-5 (S)-methyl-[1, 3 [(R)]] [DIOXAN-4-YL]-4] (R)-methyl-undeca-2, [8-DIEN-1-OL] (672296-36-5)

Guidance literature:

With sodium tetrahydroborate; In tetrahydrofuran; water; at 0 ℃; for 4h;

Reference yield: 99.0%

5 (S), 7 (S)-BIS-(TERT-BUTYL-DIMETHYL-SILANYLOXY)-1 0 (S)-[2-(4-METH OXY-BENZYL)-5 (S)-methyl-[1, 3 [(R)]] [DIOXAN-4-YL]-4] (R)-methyl-undeca-2, [8-DIEN-1-OL] (672296-36-5) + trityl chloride (76-83-5) → 4-[4 (S), 6 (S)-BIS-(TERT-BUTYL-DIMETHYL-SILANYLOXY)-1 (5), 7 (R)-dimethyl-10-trityloxy-deca-2,8-DIENYL]-2-(4-METHOXY-BENZYL)-5 S-METHYL-[1,3 (R)]dioxane (672296-37-6)

Guidance literature:

With pyridine; dmap; for 18h; Heating / reflux;

Downstream raw materials:

4-[4 (S), 6 (S)-BIS-(TERT-BUTYL-DIMETHYL-SILANYLOXY)-1 ⁽⁵⁾, 7 (R)-dimethyl-10-trityloxy-deca-2,8-DIENYL]-2-(4-METHOXY-BENZYL)-5 S-METHYL-[1,3 (R)]dioxane

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