ethyl 2-(3,5-difluorophenyl)-1,6-dihydro-1-(2-methoxyethyl)-6-oxol-5-pyrimidinecarboxylate

Base Information

Chemical Name:ethyl 2-(3,5-difluorophenyl)-1,6-dihydro-1-(2-methoxyethyl)-6-oxol-5-pyrimidinecarboxylate
CAS No.:1270001-13-2
Molecular Formula:C₁₆H₁₆F₂N₂O₄
Molecular Weight:338.311
Hs Code.:

Synonyms:ethyl 2-(3,5-difluorophenyl)-1,6-dihydro-1-(2-methoxyethyl)-6-oxol-5-pyrimidinecarboxylate

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Chemical Property of ethyl 2-(3,5-difluorophenyl)-1,6-dihydro-1-(2-methoxyethyl)-6-oxol-5-pyrimidinecarboxylate

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Technology Process of ethyl 2-(3,5-difluorophenyl)-1,6-dihydro-1-(2-methoxyethyl)-6-oxol-5-pyrimidinecarboxylate

There total 4 articles about ethyl 2-(3,5-difluorophenyl)-1,6-dihydro-1-(2-methoxyethyl)-6-oxol-5-pyrimidinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1270001-22-3
3,5-difluoro-N-(2-methoxyethyl)benzenecarboximidamide hydrochloride

: 87-13-8
diethyl 2-ethoxymethylenemalonate

: 1270001-13-2
ethyl 2-(3,5-difluorophenyl)-1,6-dihydro-1-(2-methoxyethyl)-6-oxol-5-pyrimidinecarboxylate

Guidance literature:: With sodium ethanolate; In ethanol; for 24h; Reflux;

Reference yield:

: 3,5-difluoro-N-(2-methoxyethyl)benzenecarboxamide hydrochloride

: 87-13-8
diethyl 2-ethoxymethylenemalonate

: 1270001-13-2
ethyl 2-(3,5-difluorophenyl)-1,6-dihydro-1-(2-methoxyethyl)-6-oxol-5-pyrimidinecarboxylate

Guidance literature:: With sodium ethanolate; In ethanol; for 24h; Reflux;

Reference yield:

: 64248-63-1
3,5-difluorobenzonitrile

: 1270001-13-2
ethyl 2-(3,5-difluorophenyl)-1,6-dihydro-1-(2-methoxyethyl)-6-oxol-5-pyrimidinecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: acetyl chloride / dichloromethane / 0 - 20 °C

2: methanol / 0 - 20 °C

3: sodium ethanolate / ethanol / 24 h / Reflux

With sodium ethanolate; acetyl chloride; In methanol; ethanol; dichloromethane;