3-bromo-5-fluoro-4-nitrobenzonitrile

Base Information

• Chemical Name: 3-bromo-5-fluoro-4-nitrobenzonitrile
• CAS No.: 1310918-28-5
• Molecular Formula: C₇H₂BrFN₂O₂
• Molecular Weight: 245.007
• Mol file: 1310918-28-5.mol

Synonyms:3-bromo-5-fluoro-4-nitrobenzonitrile

Chemical Property of 3-bromo-5-fluoro-4-nitrobenzonitrile

Chemical Property:

• Boiling Point: 303.1±42.0 °C(Predicted)
• Density: 1.88±0.1 g/cm3(Predicted)
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

99% ^*data from raw suppliers

3-Bromo-5-fluoro-4-nitrobenzonitrile 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-bromo-5-fluoro-4-nitrobenzonitrile

There total 2 articles about 3-bromo-5-fluoro-4-nitrobenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-amino-3-bromo-5-fluorobenzonitrile (874880-58-7) → 3-bromo-5-fluoro-4-nitrobenzonitrile (1310918-28-5)

Guidance literature:

With dihydrogen peroxide; acetic acid; In water; at 60 ℃;

Reference yield:

4-cyano-2-fluoroaniline (63069-50-1) → 3-bromo-5-fluoro-4-nitrobenzonitrile (1310918-28-5)

Guidance literature:

Multi-step reaction with 2 steps

1: bromine / acetic acid / 20 °C

2: dihydrogen peroxide; acetic acid / water / 60 °C

With dihydrogen peroxide; bromine; acetic acid; In water; acetic acid;

upstream raw materials:

4-cyano-2-fluoroaniline

4-amino-3-bromo-5-fluorobenzonitrile

Refernces