C₅₁H₆₀N₄O₃

Base Information

Chemical Name:C₅₁H₆₀N₄O₃
CAS No.:1400998-77-7
Molecular Formula:C₅₁H₆₀N₄O₃
Molecular Weight:777.062
Hs Code.:

C<sub>51</sub>H<sub>60</sub>N<sub>4</sub>O<sub>3</sub>

Synonyms:C₅₁H₆₀N₄O₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₁H₆₀N₄O₃

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Technology Process of C₅₁H₆₀N₄O₃

There total 2 articles about C₅₁H₆₀N₄O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₄H₆₈N₄O₃Si

: 1400998-77-7
C₅₁H₆₀N₄O₃

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 20 ℃; for 0.333333h;
DOI:10.1021/ol302266w

Reference yield:

: 1400998-72-2
C₄₉H₅₉IN₄O₃

: 1400998-77-7
C₅₁H₆₀N₄O₃

Guidance literature:: Multi-step reaction with 2 steps

1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / tetrahydrofuran / 15 h / 57 - 60 °C / Schlenk technique; Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.33 h / 0 - 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran; 1: |Sonogashira Cross-Coupling;
DOI:10.1021/ol302266w

Reference yield: 19.0%

: 1400998-60-8
N,N'-di(4-tert-butyl-2-iodophenyl)urea

: 1400998-77-7
C₅₁H₆₀N₄O₃

: 1400998-82-4
C₁₂₃H₁₄₄N₁₀O₇

Guidance literature:: N,N'-di(4-tert-butyl-2-iodophenyl)urea; C₅₁H₆₀N₄O₃; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 0.0833333h; Schlenk technique; Inert atmosphere;

With copper(II) sulfate; sodium L-ascorbate; In N,N-dimethyl-formamide; at 78 - 80 ℃; for 5h; Inert atmosphere; Schlenk technique;
DOI:10.1021/ol302266w