4-nitro-N-(1-phenyl-1,2,3,4-tetrahydronaphthalen-2-yl)benzenesulfonamide

Base Information

• Chemical Name: 4-nitro-N-(1-phenyl-1,2,3,4-tetrahydronaphthalen-2-yl)benzenesulfonamide
• CAS No.: 1191292-41-7
• Molecular Formula: C₂₂H₂₀N₂O₄S
• Molecular Weight: 408.478

Synonyms:4-nitro-N-(1-phenyl-1,2,3,4-tetrahydronaphthalen-2-yl)benzenesulfonamide

Chemical Property of 4-nitro-N-(1-phenyl-1,2,3,4-tetrahydronaphthalen-2-yl)benzenesulfonamide

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Technology Process of 4-nitro-N-(1-phenyl-1,2,3,4-tetrahydronaphthalen-2-yl)benzenesulfonamide

There total 3 articles about 4-nitro-N-(1-phenyl-1,2,3,4-tetrahydronaphthalen-2-yl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

1-(4-nitrobenzenesulfonyl)-2-phenethyl-3-phenylaziridine → 4-nitro-N-(1-phenyl-1,2,3,4-tetrahydronaphthalen-2-yl)benzenesulfonamide + 4-nitro-N-(1-phenyl-1,2,3,4-tetrahydronaphthalen-2-yl)benzenesulfonamide (1191292-41-7)

Guidance literature:

With copper(II) bis(trifluoromethanesulfonate); In dichloromethane; at 20 ℃; for 1.5h; optical yield given as %ee; enantioselective reaction;

DOI:10.1002/adsc.200800603

Reference yield:

1-(4-nitrobenzenesulfonyl)-2-phenethyl-3-phenylaziridine → 4-nitro-N-(1-phenyl-1,2,3,4-tetrahydronaphthalen-2-yl)benzenesulfonamide + 4-nitro-N-(1-phenyl-1,2,3,4-tetrahydronaphthalen-2-yl)benzenesulfonamide (1191292-41-7)

Guidance literature:

With copper(II) bis(trifluoromethanesulfonate); In dichloromethane; at 20 ℃; for 2h; optical yield given as %ee; enantioselective reaction;

DOI:10.1002/adsc.200800603

Reference yield:

PhINSO2(4-NO2-C6H4) + 2-phenylethylstyrene (14213-84-4,27066-35-9,70388-65-7) → 4-nitro-N-(1-phenyl-1,2,3,4-tetrahydronaphthalen-2-yl)benzenesulfonamide + 4-nitro-N-(1-phenyl-1,2,3,4-tetrahydronaphthalen-2-yl)benzenesulfonamide (1191292-41-7)

Guidance literature:

PhINSO₂(4-NO₂-C₆H₄); 2-phenylethylstyrene; With copper(II) bis(trifluoromethanesulfonate); (4R,4'R)-2,2'-(propane-2,2'diyl)bis(4-phenyl-4,5-dihydrooxazole); In dichloromethane; at 25 ℃; Molecular sieve; Inert atmosphere;

With copper(II) bis(trifluoromethanesulfonate); In Dichlorofluoromethane; optical yield given as %ee; enantioselective reaction; Inert atmosphere;

DOI:10.1002/adsc.200800603

upstream raw materials:

2-phenylethylstyrene

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