(ortho-tolyl)(1-methylimidazol-2-diphenylmethanolato)(triphenylphosphino)nickel(II)

Base Information

Chemical Name:(ortho-tolyl)(1-methylimidazol-2-diphenylmethanolato)(triphenylphosphino)nickel(II)
CAS No.:886058-75-9
Molecular Formula:C₄₂H₃₇N₂NiOP
Molecular Weight:675.432
Hs Code.:

Synonyms:(ortho-tolyl)(1-methylimidazol-2-diphenylmethanolato)(triphenylphosphino)nickel(II)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (ortho-tolyl)(1-methylimidazol-2-diphenylmethanolato)(triphenylphosphino)nickel(II)

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Technology Process of (ortho-tolyl)(1-methylimidazol-2-diphenylmethanolato)(triphenylphosphino)nickel(II)

There total 1 articles about (ortho-tolyl)(1-methylimidazol-2-diphenylmethanolato)(triphenylphosphino)nickel(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: trans-(o-tolyl)bromobis(triphenylphosphine)nickel(II)

: 30517-58-9
2-(diphenylhydroxymethyl)-1-methyl-1H-imidazole

: 886058-75-9
(ortho-tolyl)(1-methylimidazol-2-diphenylmethanolato)(triphenylphosphino)nickel(II)

Guidance literature:: With potassium methoxide; In tetrahydrofuran; (under N2, Schlenk); soln. of ligand in THF added to potassium methoxide, stirred for 12 h, solvent evapd. in vac., soln. of Ni-complex in THF added, stirred for 24 h; filtered, solvent removed in vacuo, dissolved in CH2Cl2, filtered, washed with CH2Cl2, pentane added, collected, washed with pentane, dried in vac.; elem. anal.;
DOI:10.1016/j.ica.2004.06.069