DL-N-(2-Hydroxy-2-phenylethyl)-thionobenzamid

Base Information

• Chemical Name: DL-N-(2-Hydroxy-2-phenylethyl)-thionobenzamid
• CAS No.: 26112-41-4
• Molecular Formula: C₁₅H₁₅NOS
• Molecular Weight: 257.356
• Mol file: 26112-41-4.mol

Synonyms:DL-N-(2-Hydroxy-2-phenylethyl)-thionobenzamid

Chemical Property of DL-N-(2-Hydroxy-2-phenylethyl)-thionobenzamid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of DL-N-(2-Hydroxy-2-phenylethyl)-thionobenzamid

There total 2 articles about DL-N-(2-Hydroxy-2-phenylethyl)-thionobenzamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

thiobenzoic acid (98-91-9) + 2-Amino-1-phenylethanol (7568-93-6,1936-63-6) → DL-N-(2-Hydroxy-2-phenylethyl)-thionobenzamid (26112-41-4)

Guidance literature:

With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; 1-hydroxybenzotriazol-hydrate; In dichloromethane; at 25 ℃;

DOI:10.1021/ja040093a

Reference yield:

→ DL-N-(2-Hydroxy-2-phenylethyl)-thionobenzamid (26112-41-4)

Guidance literature:

DL-2-Dimethylamino-1-phenyl-ethanol in Ae. m. Methyl-dithiobenzoat;

Reference yield: 79.0%

DL-N-(2-Hydroxy-2-phenylethyl)-thionobenzamid (26112-41-4) → 2,5-diphenyl-4,5-dihydrothiazole

Guidance literature:

With pyridine; trichlorophosphate; at 25 ℃; for 3h;

DOI:10.1021/ja040093a

upstream raw materials:

thiobenzoic acid

2-Amino-1-phenylethanol