(2-methylbutane-1,1,4-triyl)tribenzene

Base Information

Chemical Name:(2-methylbutane-1,1,4-triyl)tribenzene
CAS No.:118083-50-4
Molecular Formula:C₂₃H₂₄
Molecular Weight:300.444
Hs Code.:

Synonyms:(2-methylbutane-1,1,4-triyl)tribenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2-methylbutane-1,1,4-triyl)tribenzene

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Technology Process of (2-methylbutane-1,1,4-triyl)tribenzene

There total 9 articles about (2-methylbutane-1,1,4-triyl)tribenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 101-81-5
Diphenylmethane

: diethyl (4-phenylbutan-2-yl) phosphate

: 1530-03-6
1,1-diphenylpropane

: 118083-50-4
(2-methylbutane-1,1,4-triyl)tribenzene

Guidance literature:: Diphenylmethane; With n-butyllithium; In tetrahydrofuran; hexane; at 0 - 20 ℃; for 0.25h;

diethyl (4-phenylbutan-2-yl) phosphate; In tetrahydrofuran; hexane; at -15 ℃; for 0.25h;
DOI:10.1002/ejoc.201801596

Reference yield:

: 101-81-5
Diphenylmethane

: diphenyl (4-phenylbutan-2-yl) phosphate

: 632-50-8
1,1,2,2-tetraphenylethane

: 118083-50-4
(2-methylbutane-1,1,4-triyl)tribenzene

Guidance literature:: Diphenylmethane; With n-butyllithium; In tetrahydrofuran; hexane; at 0 - 20 ℃; for 0.25h;

diphenyl (4-phenylbutan-2-yl) phosphate; In tetrahydrofuran; hexane; at -15 ℃; for 0.25h; Overall yield = 89 %; Overall yield = 54 mg;
DOI:10.1002/ejoc.201801596

Reference yield:

: 2344-70-9
1-phenyl-3-butanol

: 118083-50-4
(2-methylbutane-1,1,4-triyl)tribenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1-methyl-1H-imidazole / dichloromethane / 2 h / 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / 0 - 20 °C

2.2: 0.25 h / -15 °C

With 1-methyl-1H-imidazole; n-butyllithium; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1002/ejoc.201801596