1-O-benzoyl 2-deoxy-4,6-O-isopropylidene-3-O--2-(octadecanoylamino)-β-D-glucopyranose

Base Information

Chemical Name:1-O-benzoyl 2-deoxy-4,6-O-isopropylidene-3-O--2-(octadecanoylamino)-β-D-glucopyranose
CAS No.:92466-94-9
Molecular Formula:C₃₈H₆₁NO₉
Molecular Weight:675.904
Hs Code.:

1-O-benzoyl 2-deoxy-4,6-O-isopropylidene-3-O-<D-1-(methoxycarbonyl)ethyl>-2-(octadecanoylamino)-β-D-glucopyranose

Synonyms:1-O-benzoyl 2-deoxy-4,6-O-isopropylidene-3-O--2-(octadecanoylamino)-β-D-glucopyranose

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Chemical Property of 1-O-benzoyl 2-deoxy-4,6-O-isopropylidene-3-O--2-(octadecanoylamino)-β-D-glucopyranose

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Technology Process of 1-O-benzoyl 2-deoxy-4,6-O-isopropylidene-3-O--2-(octadecanoylamino)-β-D-glucopyranose

There total 5 articles about 1-O-benzoyl 2-deoxy-4,6-O-isopropylidene-3-O--2-(octadecanoylamino)-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.5%

: 78397-95-2
benzyl 2-deoxy-4,6-O-isopropylidene-3-O--2-(octadecanoylamino)-β-D-glucopyranoside

: 92466-94-9
1-O-benzoyl 2-deoxy-4,6-O-isopropylidene-3-O--2-(octadecanoylamino)-β-D-glucopyranose

Guidance literature:: With pyridine; chromium(VI) oxide; acetic anhydride; In dichloromethane; at 45 ℃; for 3h;
DOI:10.1016/0008-6215(84)85404-X

Reference yield:

: 74660-47-2
benzyl 3,4,6-tri-O-acetyl-2-deoxy-2-(octadecanoylamino)-β-D-glucopyranoside

: 92466-94-9
1-O-benzoyl 2-deoxy-4,6-O-isopropylidene-3-O--2-(octadecanoylamino)-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 5 steps

1: sodium, methanol / 0.5 h / Ambient temperature

2: p-toluenesulfonic acid monohydrate / dimethylformamide; dioxane / 1 h / 40 - 45 °C

3: 1.) 50 percent sodium hydride, 3.) 2 M hydrochloric acid / 1.) 1,4-dioxane/oil, 95 deg C, 1 h, 2.) 95 deg C, 30 min

4: diethyl ether

5: 89.5 percent / chromium trioxide, pyridine, acetic anhydride / CH₂Cl₂ / 3 h / 45 °C

With pyridine; chromium(VI) oxide; hydrogenchloride; methanol; sodium; acetic anhydride; sodium hydride; toluene-4-sulfonic acid; In 1,4-dioxane; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(84)85404-X

Reference yield:

: 78397-93-0
benzyl 2-deoxy-4,6-O-isopropylidene-2-(octadecanoylamino)-β-D-glucopyranoside

: 92466-94-9
1-O-benzoyl 2-deoxy-4,6-O-isopropylidene-3-O--2-(octadecanoylamino)-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) 50 percent sodium hydride, 3.) 2 M hydrochloric acid / 1.) 1,4-dioxane/oil, 95 deg C, 1 h, 2.) 95 deg C, 30 min

2: diethyl ether

3: 89.5 percent / chromium trioxide, pyridine, acetic anhydride / CH₂Cl₂ / 3 h / 45 °C

With pyridine; chromium(VI) oxide; hydrogenchloride; acetic anhydride; sodium hydride; In diethyl ether; dichloromethane;
DOI:10.1016/0008-6215(84)85404-X