(-)-(3S,4R,6R)-3-(3',4'-dimethoxy-α-hydroxybenzyl)-4-<3'',4''-dimethoxybenzyl>butyrolactone

Base Information Edit

Chemical Name:(-)-(3S,4R,6R)-3-(3',4'-dimethoxy-α-hydroxybenzyl)-4-<3'',4''-dimethoxybenzyl>butyrolactone
CAS No.:108102-81-4
Molecular Formula:C₂₂H₂₆O₇
Molecular Weight:402.444
Hs Code.:
Mol file:108102-81-4.mol

Synonyms:(-)-(3S,4R,6R)-3-(3',4'-dimethoxy-α-hydroxybenzyl)-4-<3'',4''-dimethoxybenzyl>butyrolactone

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Chemical Property of (-)-(3S,4R,6R)-3-(3',4'-dimethoxy-α-hydroxybenzyl)-4-<3'',4''-dimethoxybenzyl>butyrolactone Edit

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Technology Process of (-)-(3S,4R,6R)-3-(3',4'-dimethoxy-α-hydroxybenzyl)-4-<3'',4''-dimethoxybenzyl>butyrolactone

There total 23 articles about (-)-(3S,4R,6R)-3-(3',4'-dimethoxy-α-hydroxybenzyl)-4-<3'',4''-dimethoxybenzyl>butyrolactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 108102-77-8
(R)-4-(3,4-dimethoxybenzyl)dihydrofuran-2(3H)-one

: 120-14-9
3,4-dimethoxy-benzaldehyde

: 78173-81-6,78215-57-3,108102-78-9,108102-81-4,144539-73-1
<(dimethoxy-3,4 phenyl)hydroxymethyl>-2 (dimethoxy-3,4 benzyl)-3 butanolide-4

Guidance literature:: With n-butyllithium; 1,1,1,3,3,3-hexamethyl-disilazane; In hexane; benzene; at 0 ℃; for 0.0666667h;
DOI:10.1016/0040-4020(89)80041-9

Reference yield: 88.0%

: 108102-77-8
(R)-4-(3,4-dimethoxybenzyl)dihydrofuran-2(3H)-one

: 120-14-9
3,4-dimethoxy-benzaldehyde

: 78173-81-6,78215-57-3,108102-78-9,108102-81-4,144539-73-1
(3S,4R)-4-(3,4-Dimethoxy-benzyl)-3-[(3,4-dimethoxy-phenyl)-hydroxy-methyl]-dihydro-furan-2-one

Guidance literature:: With 1,1,1,3,3,3-hexamethyl-disilazane; In benzene; for 0.0666667h; Ambient temperature;
DOI:10.1016/S0040-4039(00)83862-9