Ethyl 2-hydroxy-6-methoxybenzoate

Base Information

Chemical Name:Ethyl 2-hydroxy-6-methoxybenzoate
CAS No.:35030-99-0
Molecular Formula:C₁₀H₁₂O₄
Molecular Weight:196.203
Hs Code.:
Nikkaji Number:J3.104.971G

Synonyms:AKOS006295767

Suppliers and Price of Ethyl 2-hydroxy-6-methoxybenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethyl 2-hydroxy-6-methoxybenzoate

Chemical Property:

XLogP3:2.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:196.07355886
Heavy Atom Count:14
Complexity:193

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCOC(=O)C1=C(C=CC=C1OC)O

Technology Process of Ethyl 2-hydroxy-6-methoxybenzoate

There total 4 articles about Ethyl 2-hydroxy-6-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 7335-26-4
ethyl 2-methoxybenzoate

: 35030-99-0
ethyl 2-hydroxy-6-methoxybenzoate

Guidance literature:: With dipotassium peroxodisulfate; [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; trifluoroacetic acid; trifluoroacetic anhydride; at 80 ℃; for 10h;
DOI:10.1021/ol301104n

Reference yield:

: 2065-27-2
methyl 2,6-dimethoxybenzoate

: 35030-99-0
ethyl 2-hydroxy-6-methoxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 35 percent / NaBH₄, I₂ / CHCl₃ / 18 h

2: 58 percent / H₂SO₄ (d = 1.84) / 100 h / Heating

With sodium tetrahydroborate; sulfuric acid; iodine; In chloroform;